Abstract
Structural, microstructural, magnetic, electrical and magneto-transport properties of La0.7Ca0.18Ba0.12Mn0.95Sn0.05O3 manganite powders, prepared by the solid state method, were investigated. Two quenching processes were performed on the samples: quenching in air and quenching to 77 K in liquid nitrogen. X-ray diffraction patterns refinement revealed that the samples crystallized in the orthorhombic structure. The scanning electron microscopy micrographs presented granular characters. The magnetization vs temperature plot showed a paramagnetic-ferromagnetic transition. The inverse susceptibility \({\chi }^{-1}(T)\) deviation from the Curie–Weiss law revealed the existence of the phase above TC in the nitrogen-quenched sample. The hysteresis cycles reveal that the samples are ferromagnetic at 1.8 K and paramagnetic at 300 K. The resistivity curves exhibit a ferromagnetic-metallic to paramagnetic-insulating transition. The magnetoresistance increased slightly in the sample quenched to 77 K in N2.
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The datasets generated during and/or analysed during the current study are available from the corresponding author on reasonable request.
References
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Acknowledgements
This work was supported by the General Direction of Scientific Research and of Technological Development of Algeria (DGRSDT/MESRS).
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NM conceived of the presented idea. IB, FM, and NM prepared the samples. NM, FM conceived and planned the experiments. IB, FD, SPA and CT, carried out the structural, microstructural and magneto-electrical measurements. JAA and JLM carried out the magnetic measurements. IB simulated and discussed the refinement of the XRD patterns. IB, FM and NM carried out and discussed the simulation results of the magnetic and the magneto-electrical experimental data. IB, FM and NM wrote the manuscript. All authors discussed the results, contributed, and commented on the final manuscript. FM and NM supervised the project.
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Belal, I., Meriche, F., Mahamdioua, N. et al. Structural, electrical, magnetic and magnetotransport properties of La0.7Ca0.18Ba0.12Mn0.95Sn0.05O3 manganite prepared with different quenching processes. Appl. Phys. A 129, 26 (2023). https://doi.org/10.1007/s00339-022-06302-5
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DOI: https://doi.org/10.1007/s00339-022-06302-5