Abstract
The behavior of the thermally stable austenite in the ductile fracture surface layer of a grain-refined and tempered 9Ni steel broken at 77 K was studied through use of Möss-bauer spectroscopy and transmission electron microscopy. Thin foils revealing the mi-crostructural profile of the fracture surface layer were prepared by electroplating a thick pure iron layer on the fresh fracture surface, then thinning a profile sample through a combination of conventional twin-jet electropolishing and ion milling techniques. The re-sults of both Mössbauer spectroscopy and TEM studies showed that the thermally stable austenite transforms to a dislocated martensite in the deformed zone adjacent to the duc-tile fracture surface. This result suggests that transformation of the retained austenite present in tempered 9Ni steel is compatible with low temperature toughness, at least when the transformation product is a ductile martensite.
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Syn, C.K., Fultz, B. & Morris, J.W. Mechanical stability of retained austenite in tempered 9Ni steel. Metall Trans A 9, 1635–1640 (1978). https://doi.org/10.1007/BF02661946
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DOI: https://doi.org/10.1007/BF02661946