Skip to main content
SpringerLink
Log in

Electrochemical Surface X-Ray Scattering

  • Chapter
  • First Online:
Compendium of Surface and Interface Analysis

Abstract

Electrochemical surface X-ray scattering (EC-SXS) is an application of surface X-ray scattering (SXS) technique, one of the surface analysis methods, to electrochemical interfaces, i.e., electrode/electrolyte solution interfaces.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Log in via an institution

Institutional subscriptions

References

  1. Uosaki, K.: In situ real-time monitoring of geometric, electronic, and molecular structures at solid/liquid interfaces. Jpn. J. Appl. Phys. Part1 54, 030102/1–030102/14 (2015)

    Article  Google Scholar 

  2. Kondo, T., Masuda, M., Uosaki, K.: In situ SXS and XAFS measurements of electrochemical interface. In: Kumar, C.S.S.R. (eds.) X-ray and Neutron Techniques for Nanomaterials Characterization (Chap. 7), pp. 367–450. Springer, Berlin (2016)

    Google Scholar 

  3. Toney, M.F., McBreen, J.: In situ synchrotron X-ray techniques for determining atomic structure at electrode/electrolyte interfaces. Electrochem. Soc. Interface 2(Spring), 22–31 (1993)

    CAS  Google Scholar 

  4. Feidenhansl, R.: Surface-structure determination by modern X-ray physics. Surf. Sci. Rep. 10, 105–188 (1989)

    Article  CAS  Google Scholar 

  5. Wang, J., Ocko, B.M., Davenport, A.J., Isaacs, H.S.: In situ X-ray-diffraction and X-ray-reflectivity studies of the Au(111) electrolyte interface—reconstruction and anion adsorption. Phys. Rev. B 46, 10321–10338 (1992)

    Article  CAS  Google Scholar 

  6. Scherb, G., Kazimirov, A., Zegenhagen, J., Lee, T.L., Bedzyk, M.J., Noguchi, H., Uosaki, K.: In situ X-ray standing-wave analysis of electrodeposited Cu monolayers on GaAs(001). Phys. Rev. B 58, 10800–10805 (1998)

    Article  CAS  Google Scholar 

  7. Nagy, Z., You, H.: Applications of surface X-ray scattering to electrochemistry problems. Electrochim. Acta 47, 3037–3055 (2002)

    Article  CAS  Google Scholar 

  8. Tamura, K., Wang, J.X., Adzic, R.R., Ocko, B.M.: Kinetics of monolayer Bi electrodeposition on Au(111): surface X-ray scattering and current transients. J. Phys. Chem. B 108, 1992–1998 (2004)

    Article  CAS  Google Scholar 

  9. Ayyad, A.H., Stettner, J., Magnussen, O.M.: Electrocompression of the Au(111) surface layer during Au electrodeposition. Phys. Rev. Lett. 94, 066106/1-066106/4 (2005)

    Google Scholar 

  10. Krug, K., Stettner, J., Magnussen, O.M.: In situ surface X-ray diffraction studies of homoepitaxial electrochemical growth on Au(100). Phys. Rev. Lett. 96, 246101/1–246101/4

    Google Scholar 

  11. Kondo, T., Zegenhagen, J., Takakusagi, S., Uosaki, K.: In situ real-time study on potential induced structure change at Au(111) and Au(100) single crystal electrode/sulfuric acid solution interfaces by surface X-ray scattering. Surf. Sci. 631, 96–104 (2015)

    Article  CAS  Google Scholar 

  12. Kondo, T., Masuda, T., Aoki, N., Uosaki, K.: Potential-dependent structures and potential-induced structure change at Pt(111) single-crystal electrode/sulfuric and perchloric acid interfaces in the potential region between hydrogen underpotential deposition and surface oxide formation by in situ surface X-ray scattering. J. Phys. Chem. C 120, 16118–16131 (2016)

    Article  CAS  Google Scholar 

  13. Lucas, C.A., Cormack, M., Gallagher, M.E., Brownrigg, A., Thompson, P., Fowler, B., Gründer, Y., Roy, J., Stamenković, V., Marković, N.M.: From ultra-high vacuum to the electrochemical interface: x-ray scattering studies of model electrocatalyst. Faraday Discuss. 140, 41–58 (2008)

    Article  CAS  Google Scholar 

  14. Tripkovic, D.V., Strmcnik, D., van der Vliet, D., Stamenković, V., Marković, N.M.: The role of anions in surface electrochemistry. Faraday Discuss. 140, 25–40 (2008)

    Article  CAS  Google Scholar 

  15. Marković, N.M., Ross Jr., P.N.: Surface science studies of model fuel cell electrocatalysts. Surf. Sci. Rep. 45, 117–229 (2002)

    Article  Google Scholar 

  16. Sisson, N., Gründer, Y., Lucas, C.A.: Structure and stability of underpotentially deposited Ag on Au(111) in alkaline electrolyte. J. Phys. Chem. C 120, 16100–16109 (2016)

    Article  CAS  Google Scholar 

  17. Kondo, T., Morita, J., Okamura, M., Saito, T., Uosaki, K.: In situ structural study on underpotential deposition of Ag on Au(111) electrode using surface X-ray scattering technique. J. Electroanal. Chem. 532, 201–205 (2002)

    Article  CAS  Google Scholar 

  18. Uosaki, K., Morita, J., Katsuzaki, T., Takakusagi, S., Tamura, K., Takahasi, M., Mizuki, J., Kondo, T.: In situ electrochemical, electrochemical quartz crystal microbalance, scanning tunneling microscopy, and surface X-ray scattering studies on Ag/AgCl reaction at the underpotentially deposited Ag bilayer on the Au(111) electrode surface. J. Phys. Chem. C 115, 12471–12482 (2011)

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Division of Chemistry, Graduate School of Humanities and Sciences, Ochanomizu University, Tokyo, Japan

    Toshihiro Kondo

Authors
  1. Toshihiro Kondo
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Toshihiro Kondo .

Editor information

Editors and Affiliations

  1. Tokyo, Japan

    The Surface Science Society of Japan

Rights and permissions

Reprints and permissions

Copyright information

© 2018 Springer Nature Singapore Pte Ltd.

About this chapter

Check for updates. Verify currency and authenticity via CrossMark

Cite this chapter

Kondo, T. (2018). Electrochemical Surface X-Ray Scattering. In: The Surface Science Society of Japan (eds) Compendium of Surface and Interface Analysis. Springer, Singapore. https://doi.org/10.1007/978-981-10-6156-1_18

Download citation

Publish with us

Policies and ethics

Search

Navigation