Summary
FT-ICR mass spectrometry may be considered as a new analytical method for the diagnosis of soils contaminated with organic compounds. Optimization of the parameters of an ICR events sequence governing an analysis is presented. Coupling the use of the solid phase microextraction technique to FT-ICR mass spectrometry makes it possible to extract and analyze some of the pollutants from “synthetic” soils spiked with PAHs, without solvent extraction.
Kurzfassung
Die FT-ICR-Massenspektrometrie kommt als neue Analysemethode zur Diagnose von mit organischen Substanzen belasteten Böden in Betracht. Eine Parameteroptimierung zu einer Folge von die Analyse bestimmenden ICR-Ereignissen wird vorgestellt. Die Verknüpfung der Flüssigphasen-Mikroextraktionstechnik mit der FT-ICR-Massenspektrometrie ermöglicht Extraktion und Analyse verschiedener künstlich (unter Hinzufugung von PAKs) kontaminierter Böden, ohne Einsatz von Solvent-Extraktionsverfahren.
Résumé
La spectrométrie de masse FT-ICR peut être envisagée comme une nouvelle methode analytique lors du diagnostic des sols contaminés par des composés organiques. L’optimisation des paramétres d’une séquence d’événements ICR gouvernant une analyse est présentée. Le couplage de 1a technique d’extraction solid phase microextraction au spectrométre de masse FT-ICR permet d’extraire et d’analyser certains polluants de sols contaminés “synthetique” (avec adjonetion de PAH) sans utilisation de solvants d’extraction.
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© 1995 Kluwer Academic Publishers
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Boisson, P., Gal, JF., Maria, PC., Pagliardini, A. (1995). Volatile Organic Compounds and Polycyclic Aromatic Hydrocarbons in Soils Polluted by Industrial Activities: Fourier Transform Ion Cyclotron Resonance Mass Spectrometry (FT-ICR) as an Investigation Tool. In: Van Den Brink, W.J., Bosman, R., Arendt, F. (eds) Contaminated Soil ’95. Soil & Environment, vol 5. Springer, Dordrecht. https://doi.org/10.1007/978-94-011-0415-9_119
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DOI: https://doi.org/10.1007/978-94-011-0415-9_119
Publisher Name: Springer, Dordrecht
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