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Study of ZrO2 Coatings by Thermoanalytical and Fourier Spectroscopic Methods

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Progress in Fourier Transform Spectroscopy

Part of the book series: Mikrochimica Acta Supplement ((MIKROCHIMICA,volume 14))

  • 23 Accesses

Abstract

The formation mechanism of ZrO2 — used for the stabilization of electrocatalytic thin films — from ZrOCl2·8H2O precursor was followed as the function of the firing temperature for the powder form as well as for the form of a thin film deposited on a titanium support. It was found that an intramolecular hydrolysis takes place upon heating, resulting in the liberation of hydrogen chloride. XRD, FT-IR and FT-Raman investigations revealed that polymorphism occurs in the oxide film. The upper surface of the film is of tetragonal structure, while the bulk is of cubic form stabilized by TiO2 formed by oxidation of the support.

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References

  1. A. De Battisti, G. Battaglin, A. Benedetti, J. Kristóf, J. Liszi, Chimia 1995, 49, 17.

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  2. J. Kristóf, J. Mink, A. De Battisti, J. Liszi, Electrochim. Acta 1994, 39, 1531.

    Article  Google Scholar 

  3. J. Mink, J. Kristóf, A. De Battisti, S. Daolio, Cs. Nerneth, Surf. Sci. 1995, 335, 252.

    Article  CAS  Google Scholar 

  4. C. M. Phillippi, K. S. Mazdiyasni, J. Am. Ceram. Soc. 1971, 54, 254.

    Article  CAS  Google Scholar 

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Author information

Authors and Affiliations

  1. Department of Analytical Chemistry, University of Veszprém, P. O. Box 158, H-8201, Veszprém, Hungary

    J. Mihály, J. Kristóf & J. Mink

  2. Dipartimento di Chimica, Università di Ferrara, via L. Borsari 46, I-44100, Ferrara, Italy

    L. Nanni, D. Patracchini & A. De Battisti

Authors
  1. J. Mihály
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  2. J. Kristóf
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  3. J. Mink
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  4. L. Nanni
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  5. D. Patracchini
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  6. A. De Battisti
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Editor information

Editors and Affiliations

  1. Department of Analytical Chemistry, University of Veszprém, Veszprém, Hungary

    János Mink

  2. Institute of Isotopes, Hungarian Academy of Sciences, Budapest, Hungary

    János Mink

  3. Central Research Institute of Chemistry, Hungarian Academy of Sciences, Budapest, Hungary

    Gábor Keresztury

  4. Institut für Analytische Chemie, Technische Universität Wien, Wien, Austria

    Robert Kellner

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© 1997 Springer-Verlag Wien

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Cite this paper

Mihály, J., Kristóf, J., Mink, J., Nanni, L., Patracchini, D., De Battisti, A. (1997). Study of ZrO2 Coatings by Thermoanalytical and Fourier Spectroscopic Methods. In: Mink, J., Keresztury, G., Kellner, R. (eds) Progress in Fourier Transform Spectroscopy. Mikrochimica Acta Supplement, vol 14. Springer, Vienna. https://doi.org/10.1007/978-3-7091-6840-0_157

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  • DOI: https://doi.org/10.1007/978-3-7091-6840-0_157

  • Publisher Name: Springer, Vienna

  • Print ISBN: 978-3-211-82931-8

  • Online ISBN: 978-3-7091-6840-0

  • eBook Packages: Springer Book Archive

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