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In situ Characterisation of Practical Heterogeneous Catalysts

  • Chapter
Basic Principles in Applied Catalysis

Part of the book series: Springer Series in Chemical Physics ((CHEMICAL,volume 75))

Abstract

In situ methods are considered as a curiosity within the standard methodology of practical catalyst characterisation. The methods are not commercially available and need to be adapted and validated for each specific problem. The great advantage of these methods is, however, that they deliver immediately relevant characteristics of the working state of a heterogeneous catalyst and allow justified structure-function relations to be deduced. To achieve this it is essential that the experiments are planned and conducted in such a way that the proven to be active state of the catalyst is investigated. This can only be ascertained if simultaneous kinetic and spectroscopic data are acquired. The contribution lists a selection of methods with their main characteristics that allows to choose from the wide spectrum of information those that are most relevant for the given problem. A tabulated selection of case studies from the literature gives some insight in the current practice.

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  1. Fritz-Haber-Institut der MPG, Faradayweg 4-6, 14195, Berlin, Germany

    Robert Schlögl

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    Manfred Baerns

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Schlögl, R. (2004). In situ Characterisation of Practical Heterogeneous Catalysts. In: Baerns, M. (eds) Basic Principles in Applied Catalysis. Springer Series in Chemical Physics, vol 75. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-05981-4_9

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