Coulometrische Methoden

Gründler, P.

doi:10.1007/978-3-642-60430-0_2

P. Gründler¹³

Part of the book series: Analytiker-Taschenbuch ((ANALYTIKERTB,volume 15))

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Zusammenfassung

Unter Coulometrie wird in der Chemie allgemein das Prinzip verstanden, aus der Messung einer Ladungsmenge (gemessen in der Einheit Coulomb gleich Amperesekunde) auf die Stoffmenge chemischer Bestandteile zu schließen. In der analytischen Chemie sind coulometrische Methoden im engeren Sinne solche Elektrolyseprozesse, bei denen dafür gesorgt wird, daß ein annähernd vollständiger Umsatz, d.h. eine nahezu 100 prozentige Reduktion bzw. Oxydation der zu bestimmenden Spezies stattfindet. Dies ist die Voraussetzung für eine sinnvolle Auswertung der Messungen. Diese ursprüngliche Bindung des Begriffes an die Notwendigkeit des vollständigen Umsatzes hat dazu geführt, daß häufig auch in anderem Zusammenhang von coulometrischer Arbeitsweise gesprochen wird, wenn eine „erschöpfende Elektrolyse" gemeint ist. Charakteristisch für diese Arbeitsweise ist ein möglichst großer Wert des Verhältnisses von Elektrodenoberfläche zu Lösungsvolumen. Dies liefert z.B. eine Unter-scheidungsmöglichkeit zwischen amperometrischen und coulometrischen Detektoren.

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Einleitung zur Elektrotechnik

Spezielle elektrische Temperaturmessverfahren

Die Grundgleichungen des elektrostatischen Feldes

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Fachbereich Chemie, Abt. Analytik und Umweltchemie, Universität Rostock, Buchbinderstr. 9, D-18051, Rostock, Deutschland
P. Gründler

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Bismarckstr. 4, D-69469, Weinheim, Deutschland
Helmut Günzler
Chemie and Abfallanalytik Technische Univerität, Hagenring 30, D-38106, Braunscweig, Deutschland
A. Müfit Bahadir (Inst. f. Ökolog.) (Inst. f. Ökolog.)
Fachbereich Chemie, Universität Leipzig, Talstr. 35, D-04103, Leipzig, Deutschland
Rolf Borsdorf
Institut für Anorganische und Analytische Chemie, Chemische Fakultät Friedrich-Schiller-Universität, Lessingstr. 8, D-07743, Jena, Deutschland
Klaus Danzer
Institut Fresenius, Im Maisel, D-65232, Taunusstein, Deutschland
Wilhelm Fresenius
Inst. f. Lebenmittelwissenschaft und Lebensmittelchemie der Rheinischen, Friedrich-Wilhelms-Universität Bonn, Endenicher Allee 11–13, D-53115, Bonn, Deutschland
Rudolf Galensa
Weimarerstr. 69, D-67071, Ludwigshafen, Deutschland
Walter Huber
Institut für Spektrochemie und Angewandte Spektroskopie, Postfach 101352, D-44013, Dortmund, Deutschland
Michael Linscheid
Core Div. Quality Assurance, Boehringer Ingelheim GmbH, D-55216, Ingelheim/Ruhr, Deutschland
Ingo Lüderwald
Inst. f. Analyt. u. Anorg. Chemie, TU Clausthal-Zellerfeld, Paul-Ernst-Str. 4, D-38678, Clausthal-Zellerfeld, Deutschland
Georg Schwedt
Institut für Spektrochemie and angewandte Spektroskopie, Postfach 10 13 52, D-44013, Dortmund, Deutschland
Günter Tölg
Robert-Bosch-Krankenhaus, Auerbachstr. 110, D-70376, Stuttgart, Deutschland
Hermann Wisser

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Gründler, P. (1997). Coulometrische Methoden. In: Günzler, H., et al. Analytiker-Taschenbuch. Analytiker-Taschenbuch, vol 15. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-60430-0_2

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Einleitung zur Elektrotechnik

Spezielle elektrische Temperaturmessverfahren

Die Grundgleichungen des elektrostatischen Feldes

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Einleitung zur Elektrotechnik

Spezielle elektrische Temperaturmessverfahren

Die Grundgleichungen des elektrostatischen Feldes

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