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Selective Extraction and Recovery of Rare Earth Metals (REMs) from NdFeB Magnet Grinding Sludge

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Extraction 2018

Abstract

Grinding sludge from the sintered neodymium-iron -boron (NdFeB) magnets production process was enriched with critical rare earth elements (neodymium, dysprosium and praseodymium), which can be up to 30% in the magnets . The demand of NdFeB magnets are simultaneously growing. Therefore, rare earths recovered from waste residue would reduce the demand of rare earth elements from primary sources. In this study, the feasibility of recycling rare earths through a hydrometallurgical process was investigated. The selective leaching of Nd from grinding sludge can successfully raise the rare earths concentration to 70%. The necessity of an oxidation pretreatment to improve the selectivity between Nd and Fe will be described.

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References

  1. Yang Y, Walton A, Sheridan R, Güth K, Gauß R, Gutfleisch O, Buchert M, Steenari BM, Van Gerven Y, Jones PT, Binnemans K (2017) REE recovery from End-of-Life NdFeB permanent magnet scrap: a critical review. J Sustain Metall 3:122–149

    Article  Google Scholar 

  2. Firdaus M, Rhamdhani MA, Durandet Y (2016) Review of high-temperature recovery of rare earth (Nd/Dy) from magnet waste. J Sustain Metall 2:276–295

    Article  Google Scholar 

  3. Lee CH, Chen YJ, Liao CH, Popuri SR, Tsai SL, Hung CE (2013) Selective leaching process for neodymium recovery from scrap Nd-Fe-B magnet, metall. Mater Trans A 44A:5825–5833

    Article  Google Scholar 

  4. Yoon HS, Kim CJ, Chung KW, Lee JY, Shin SM, Lee SJ, Joe AR, Lee SI, Yoo SJ (2014) Leaching kinetics of neodymium in sulfuric acid of rare earth elements (REE) slag concentrated by pyrometallurgy from magnetite ore. Korean J Chem Eng 31:1766–1772

    Article  CAS  Google Scholar 

  5. Onal MAR, Borra CR, Guo M, Blanpain B, Gerven TV (2017) Hydrometallurgical recycling of NdFeB magnets: complete leaching, iron removal and electrolysis. J. Rare Earth. 35:574–584

    Article  CAS  Google Scholar 

  6. Li Y, Xu S (2016) Hydrothermal synthesis of lanthanide (hydr)oxide micro/nanorods in presence of tetrabutylammonium hydroxide. J Rare Earth 34:618–625

    Article  CAS  Google Scholar 

  7. David AA (ed) (2016) Sustainable inorganic chemistry. Wiley, New York

    Google Scholar 

  8. Jeon SH, Nam K, Yoon HY, Kim YI, Cho DW, Sohn Y (2017) Hydrothermal synthesis of Nd2O3 nanorods. Ceram Int 43(1B):1193–1199

    Article  CAS  Google Scholar 

  9. Zawadzki M, Kepi´nski L (2004) Synthesis and characterization of neodymium oxide nanoparticles. J Alloys Compd, 380:255–259

    Article  CAS  Google Scholar 

  10. Ekthammathat N, Phuruangrat A, Kuntalue B, Thongtem S, Thongtem T (2015) Preparation of neodymium hydroxide nanorods and neodymium oxide nanorods by a hydrothermal method Dig J Nanomater Biostruct. 10(2):715–719

    Google Scholar 

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Acknowledgements

The authors would like to thank the Department of Primary Industries and Mines, Ministry of Industry of Thailand for financial support under grant number 23/2560. Suranaree University of Technology, The Center of Scientific and Technological Equipment, and Synchrotron Light Research Institute of Thailand are acknowledged for providing the instrumental analysis.

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Correspondence to Waraporn Piyawit .

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© 2018 The Minerals, Metals & Materials Society

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Piyawit, W. et al. (2018). Selective Extraction and Recovery of Rare Earth Metals (REMs) from NdFeB Magnet Grinding Sludge. In: Davis, B., et al. Extraction 2018. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-319-95022-8_202

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