Abstract
A new method has been worked out which allows the implementation of a special heating program according to which the temperature of the sample is rapidly increased so long as no changes occur in it, while it ensures nearly isothermal conditions when reactions connected with weight change are taking place. Authors succeeded furtheron in establishing a self generated atmosphere in the surroundings of the solid phase with the help of a sample holder deviced recently. According to the new technique the thermal decomposition of the sample can be investigated under quasi isothermal and quasi isobaric, consequently under quasi equilibrium conditions.
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References
F. Paulik, J. Paulik and L. Erdey, Z.Anal.Chem. 160, 241 /1958/
F. Paulik, J. Paulik and L. Erdey, Talanta 13, 1405 /1966/
J. Paulik and F. Paulik, Anal.Chim.Acta, in the press
P. D. Garn and J.E. Kessler, Anal.Chem. 32, 1563 /1960/
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© 1972 Springer Basel AG
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Paulik, F., Paulik, J. (1972). Quasi Isothermal Thermogravimetry. In: Wiedemann, H.G. (eds) Advances in Instrumentation. Birkhäuser, Basel. https://doi.org/10.1007/978-3-0348-7413-7_14
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DOI: https://doi.org/10.1007/978-3-0348-7413-7_14
Publisher Name: Birkhäuser, Basel
Print ISBN: 978-3-0348-7415-1
Online ISBN: 978-3-0348-7413-7
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