Skip to main content

Metallurgical Mechanisms upon Stress Relaxation Annealing of the AD730TM Superalloy

  • Conference paper
  • First Online:
Superalloys 2020

Abstract

Fine microstructural analyses have been performed to identify the microstructural mechanisms controlling stress relaxation during aging heat treatment of AD730TM disk superalloy. Morphological evolution of the hardening γ′ precipitates and plastic activity occur during relaxation tests. For a 500 MPa initial stress, the relaxation test shows atypical behavior with sluggish relaxation in the first hours and then a faster one. To understand this atypical behavior, isothermal dilatometry tests were used to decouple the effects of stress and temperature. The latter revealed a contraction of the specimen when subjected to a constant temperature. This contraction induces a tendency for an increase in stress during the relaxation test to meet the imposed condition of constant total deformation. Relaxation is then controlled by the competition between the classical relaxation mechanisms (vacancy diffusion and/or dislocation gliding) which tend to lower the stress and the contraction of the specimen which tends to increase the stress during the test.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 349.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 449.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 449.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Similar content being viewed by others

References

  1. Pollock T.M. and Tin S. (2006), Nickel-based superalloys for advanced turbine engines: chemistry, microstructure and properties. J. Propuls. Power, 22: 361–374.

    Google Scholar 

  2. Reed R.C. (2006) The Superalloys Fundamental and Applications, Cambridge University Press, Cambridge.

    Google Scholar 

  3. Devaux A. et al. (2010) Properties of New C&W Superalloys for High Temperature Disk Applications, Paper presented at the 7th International Symposium on Superalloy 718 and Derivatives, TMS: Warrendale, PA, USA, 223–235, 10–13 October 2010.

    Google Scholar 

  4. Devaux A. et al. (2011) Development of New C&W Superalloys for High Temperature Disk Applications, Adv. Mater. Res., 278: 405–410.

    Google Scholar 

  5. Lee D. and Hart E. W. (1971) Stress relaxation and mechanical behavior of metals, Metall. Trans., 2: 1245–1248.

    Google Scholar 

  6. Semiatin, S.L. et al. (2019) Effect of Test Method on Stress-Relaxation Behavior of Alloy 718, Metall. Mater. Trans. A, 50: 1397–1408.

    Google Scholar 

  7. Qin H. et al. (2019) Study of precipitation-assisted stress relaxation and creep behavior during the ageing of a nickel-iron superalloy, Mater. Sci. Eng. A, 742: 493–500.

    Google Scholar 

  8. Rahimi S. King M. and Dumont Ch. (2017) Stress relaxation behavior in IN718 nickel based superalloy during ageing heat treatments, Mater. Sci. Eng. A, 708: 563–573.

    Google Scholar 

  9. Nazmy M. and Gerdes C. (2011) The relaxation behavior of high Chromium - Ni base superalloys, Adv. Mater. Res., 278: 321–326.

    Google Scholar 

  10. Gabb T. et al. (2004) Stress Relaxation in Powder Metallurgy Superalloy Disks, TMS letters, 1:115–116.

    Google Scholar 

  11. Rist M.A. et al. (2006) Residual stresses in a quenched superalloy turbine disc: measurements and modeling, Metall. Mater. Trans. A, 37 (2): 459–467.

    Google Scholar 

  12. Aba-Perea P.E. et al. (2016) In-situ residual stress analysis during annealing treatments using neutron diffraction in combination with a novel furnace design, Mater. Des., 110: 925–931.

    Google Scholar 

  13. Zhang R.Y. et al. (2020) Evolution of lattice spacing of gamma double prime precipitates during aging of polycrystalline Ni-base superalloys: An In Situ investigation. Metall. Mater. Trans. A, 51: 574–585.

    Google Scholar 

  14. Collins D.M. et al. (2013) Lattice misfit during ageing of a polycrystalline nickel-base superalloy. Acta Mater., 61: 7791–7804.

    Google Scholar 

  15. Devaux A. et al. (2014) Effect of aging heat-treatment on mechanical properties of AD730TM superalloy, Paper presented at the 8th International Symposium on Superalloy 718 and Derivatives, TMS: Warrendale, PA, USA, 521–535, 28 September–1 October 2014.

    Google Scholar 

  16. Morin P. et al. (1979) Electron–channeling imaging in scanning electron microscopy, Philos. Mag. 40(4): 511–524.

    Google Scholar 

  17. Wang Y. et al. (2016) Stress relaxation behavior and mechanism of AEREX350 and Waspaloy superalloys, Mater. Sci. Eng. A, 678:10–22.

    Google Scholar 

  18. Jiang H. et al. (2018) Stress Relaxation Behavior Comparison of Typical Nickel-Base Superalloys for Fasteners, Paper presented at the 9th International Symposium on Superalloy718 and Derivatives: Energy, Aerospace, and Industrial Applications, TMS: Pittsburgh, PA, USA, 789–804, 3–6 June 2018.

    Google Scholar 

  19. Laurence A. et al (2014) Impact of the solution cooling rate and of thermal aging on the creep properties of the new cast & wrought René 65 Ni-based superalloys, Superalloy 718 and Derivatives, 333–348.

    Google Scholar 

  20. Mao J. et al. (2002) Cooling precipitation and strengthening study in powder metallurgy superalloy René88DT, Mater. Sci. Eng., 332(1):318–329.

    Google Scholar 

  21. Gadaud P. (2015) Elastic properties characterization by means of the dynamic resonant technique, Materials Characterization – Modern Methods and Applications, Ed N. Ranganathan, Stanford Publisher, Chapter 9.

    Google Scholar 

  22. Mrozowski N. et al. (2020) Aging of γ′ precipitates at 750 °C in the nickel-based superalloy AD730TM: A thermally or thermos-mechanically controlled process? Metals2020, 10, 426.

    Google Scholar 

  23. Pettinati-Sturmel F. et al. (2019) Creep behavior in the new AD730TM nickel-based disk superalloy – Influence of aging heat treatment and local chemical fluctuations, Mater. Sci. Eng. A, 754:9–17.

    Google Scholar 

  24. Li L. et al. (2020) Understanding the effetcs of alloy chemistry and microstructure on the stress relaxation behavior of Ni-base superalloys, 14th International Symposium on Superalloys 2020, 13–17 September 2020.

    Google Scholar 

  25. Thébaud L. (2017) Etude des relations entre microstructure et propriétés mécaniques du nouveau superalliage base nickel AD730™, Ph.D Thesis, École Nationale Supérieure de Mécanique et d’Aérotechnique, Poitiers, France.

    Google Scholar 

  26. Nabarro F. R. N. and Villiers F., (1995), Physics Of Creep And Creep-Resistant Alloys, CRC Press.

    Google Scholar 

  27. Laurence A. (2016) Impact du sur-vieillissement métallurgique sur le comportement et la durabilité du superalliage base nickel René 65, Ph.D Thesis, École Nationale Supérieure de Mécanique et d’Aérotechnique, Poitiers, France.

    Google Scholar 

  28. Billot T. (2010) Comportement et endommagement en fatigue et fatigue-fluage à haute température de différents états microstructuraux du superalliage base-nickel Udimet 720, Ph.D Thesis, École Nationale Supérieure de Mécanique et d’Aérotechnique, Poitiers, France.

    Google Scholar 

  29. Galindo-Nava E. et al. (2015) On the prediction of the yield stress of unimodal and multimodal γ Nickel-base superalloys, Acta Mater., 98: 377–390.

    Google Scholar 

  30. Thébaud L. et al. (2018) Is there an optimal grain size for creep resistance in Ni-based disk superalloys, Mater. Sci. Eng. A, 716:274–283.

    Google Scholar 

  31. Viswanathan G.B. et al. (2005) Investigation of creep deformation mechanisms at intermediate temperatures in René 88 DT, Acta Mater., 53:3041–3057.

    Google Scholar 

  32. Tiley J. et al. (2010) Evaluation of gamma prime volume fractions and lattice misfits in a nickel base superalloy using the external standard X-ray diffraction method, Mater. Sci. Eng. A, 528:32–36.

    Google Scholar 

  33. Jackson M.P. and Reed R.C. (1999) Heat treatment of UDIMET 720 Li: the effect of microstructure on properties, Mater. Sci. Eng. A, 259:85–97.

    Google Scholar 

  34. Dubiez-Le Goff S. et al. (2004) Effect of the microstructure on the creep behavior of PM Udimet 720 superalloy - experiments and modeling, Mater. Sci. Eng. A, 387 – 389:599–603.

    Google Scholar 

  35. Furrer D.U. and Fecht H.J. (1999) γ′ formation in superalloy U720LI, Scr. Mater., 40:1215–1220.

    Google Scholar 

  36. Flageolet B. (2005) Effets du vieillissement du superalliage base nickel pour disques de turbines N18 sur sa durabilité en fatigue et en fatigue-fluage à 700 °C, Ph.D Thesis, École Nationale Supérieure de Mécanique et d’Aérotechnique, Poitiers, France.

    Google Scholar 

  37. Bhowal P.R., Wright E.F. and Raymond E.L. (1990) Effects of Cooling Rate and γ′ Morphology on Creep and Stress-Rupture Properties of a Powder Metallurgy Superalloy, Metall. Mater. Trans. A, 21:1709–1717.

    Google Scholar 

  38. Jackson M.P. and Reed R.C. (1999) Heat treatment of UDIMET 720 Li: the effect of microstructure on properties, Mater. Sci. Eng. A, 259 (1):85–97.

    Google Scholar 

  39. Locq D. et al. (2000) Optimisation of the mechanical properties of a New PM Superalloy for Disk Applications, Paper presented at Superalloys 2000, TMS: Warrendale, PA, USA, 395 – 403, 17–21 September 2000.

    Google Scholar 

  40. Locq D. et al. (2004) On the Role of Tertiary γ′ Precipitates in the Creep Behaviour at 700 °C of a PM Disk Superalloy, Paper presented at Superalloys 2004, TMS: Warrendale, PA, USA, 179–187, 19–23 September 2004.

    Google Scholar 

  41. Poirier J. (1985) Diffusion creep, grain-boundary sliding and superplasticity, In Creep of Crystals: High-Temperature Deformation Processes in Metals, Ceramics and Minerals. Cambridge: Cambridge University Press. 194–212.

    Google Scholar 

Download references

Acknowledgements

This work received financial support from the French Agency for Scientific Research (ANR) and from the Safran Group via the industrial chair ANR-Safran OPALE.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Malik Durand .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2020 The Minerals, Metals & Materials Society

About this paper

Check for updates. Verify currency and authenticity via CrossMark

Cite this paper

Durand, M., Cormier, J., Villechaise, P., Franchet, JM., Dumont, C., Bozzolo, N. (2020). Metallurgical Mechanisms upon Stress Relaxation Annealing of the AD730TM Superalloy. In: Tin, S., et al. Superalloys 2020. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-030-51834-9_53

Download citation

Publish with us

Policies and ethics