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Microstructural Development in Pb-Sn Alloys Subjected to High-Gravity during Controlled Directional Solidification

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Materials Processing in High Gravity
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Abstract

Research conducted over the past three decades has suggested that solidification processing of metals and alloys in a centrifuge can lead to enhanced materials properties.1-11 With the potential of such processing demonstrated, there exists a need for quantitative data gathered under controlled solidification conditions. To this end, a centrifuge, dedicated to materials research, was constructed within the Materials Science and Engineering Department at Vanderbilt University. This has since been employed to investigate the effect of a high-gravity environment on microstructural development of Pb- 50 wt pct Sn alloys during controlled directional solidification.

For otherwise constant solidification processing conditions of composition, growth rate, and temperature gradient, centrifugation caused the primary dendrite arm spacing to decrease significantly. The secondary dendrite arm spacing, the eutectic spacing, and the primary dendrite trunk diameters exhibited no change with increasing gravity level.

These results are discussed in terms of suppressing convection in the bulk liquid and/or modification of the solute-enriched liquid layer about the dendrite tips. Work in progress to directly visualize effects attributed to enhanced gravity is discussed.

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References

  1. P.J. Shlichta and R.E. Knox, J. Cryst. Growth 3-4:808 (1968).

    Article  CAS  Google Scholar 

  2. G. Müller, E. Schmidt and P. Kyr, J. Cryst. Growth 49:387 (1980).

    Article  Google Scholar 

  3. G. Müller and G. Neuman, J. Cryst. Growth 59:548 (1982).

    Article  Google Scholar 

  4. G. Müller and G. Neuman, J. Cryst. Growth 63:58 (1983).

    Article  Google Scholar 

  5. W.E. Langlois, J. Cryst. Growth 63:67 (1983).

    Article  CAS  Google Scholar 

  6. G. Müller, G. Neuman, and W. Weber, J. Cryst. Growth 70:78 (1984).

    Article  Google Scholar 

  7. G. Müller, J. Cryst. Growth 99:1242 (1990).

    Article  Google Scholar 

  8. W. Weber, G. Neuman and G. Müller, J. Cryst. Growth 100:145 (1990).

    Article  CAS  Google Scholar 

  9. H. Rodot, L.L. Regel and A.M. Turtchaninov, J. Cryst. Growth 104:280 (1990).

    Article  CAS  Google Scholar 

  10. B.T. Murray, S.R. Coriell and G.B. McFadden, J. Cryst. Growth 110:713 (1991).

    Article  Google Scholar 

  11. L.L. Regel, M. Rodot and W.R. Wilcox, eds., “Material Processing in High Gravity,” (1992).

    Google Scholar 

  12. M. McLean. “Directionally Solidified Materials for high Temperature Service,” The Metals Society (1983).

    Google Scholar 

  13. J.D. Verhoeven, J.T. Mason and R. Trivedi, Metall. Transactions A. 17A:991 (1986).

    Article  CAS  Google Scholar 

  14. C. Battaile, Masters Thesis, Vanderbilt University, Dept. of Materials Science and Engineering (1992).

    Google Scholar 

  15. C. Battaile, R.N. Grugel, A.B. Hmelo and T.G. Wang in: “Microstructural Design by Solidification Processing,” E. J. Lavernia and N.N. Gungor, eds., The Minerals, Metals and Materials Society (1992) pp 161–172.

    Google Scholar 

  16. R.N. Grugel, Materials Characterization 28:213 (1992).

    Article  CAS  Google Scholar 

  17. C. Battaile, R.N. Grugel, A.B. Hmelo and T.G. Wang: Submitted to Metallurgical Trans. A.

    Google Scholar 

  18. D.J. Allen and J.D. Hunt, Metall. Transactions A. 10A:1389 (1979).

    Article  CAS  Google Scholar 

  19. T. Okamoto, K. Kishitake and I. Besso, J. Cryst. Growth 29:131 (1975).

    Article  CAS  Google Scholar 

  20. T. Huang, D. Lu and Y. Zhou, Acta. Astro 17:997 (1988).

    Article  CAS  Google Scholar 

  21. J.D. Hunt, “Solidification and Casting of Metals,” Book 192, The Metals Society, London (1979) pp 3–9.

    Google Scholar 

  22. J. Liu, Scripta Met. 26:179 (1992).

    Article  CAS  Google Scholar 

  23. G. Frohberg, K.H. Kraatz and H. Wever in: “Scientific Results of the German Spacelab Mission D1,” P.R Sahm, R. Jensen and M.H. Keller, eds., WPF, (1986) pp 144–151.

    Google Scholar 

  24. W. Kurz and D.J. Fisher, Acta Metall. 29:11 (1981).

    Article  CAS  Google Scholar 

  25. R. Trivedi, Metall. Transactions A. 15A:977 (1984).

    Article  CAS  Google Scholar 

  26. V. Laxmanan, J. Cryst. Growth 83:391 (1987).

    Article  CAS  Google Scholar 

  27. W. Kurz and R.N. Grugel. “Materials Science Forum,” Trans Tech. Publications, Switzerland (1991) pp 185–204.

    Google Scholar 

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Liya L. Regel William R. Wilcox

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© 1994 Springer Science+Business Media New York

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Grugel, R.N., Hmelo, A.B., Battaile, C.C., Wang, T.G. (1994). Microstructural Development in Pb-Sn Alloys Subjected to High-Gravity during Controlled Directional Solidification. In: Regel, L.L., Wilcox, W.R. (eds) Materials Processing in High Gravity. Springer, Boston, MA. https://doi.org/10.1007/978-1-4615-2520-2_11

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  • DOI: https://doi.org/10.1007/978-1-4615-2520-2_11

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4613-6073-5

  • Online ISBN: 978-1-4615-2520-2

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