Skip to main content

Abstract

In our rapidly expanding technology, the scientist today is more frequently required to observe and correctly explain phenomena occurring on a micrometer (μm) and submicrometer scale. The electron microprobe and scanning electron microscope are two powerful instruments which permit the characterization of heterogeneous materials and surfaces on such a local scale. In both instruments, the area to be examined is irradiated with a finely focused electron beam, which may be static, or swept in a raster across the surface of the specimen. The types of signals which are produced when the focused electron beam impinges on a specimen surface include secondary electrons, backscattered electrons, characteristic x-rays, Auger electrons, and photons of various energies. They are obtained from specific emission volumes within the sample and are used to measure many characteristics of the sample (composition, surface topography, crystallography, etc.).

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 84.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 109.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. A. N. Broers, in Scanning Electron Microscopy/1974, IITRI, Chicago, Illinois (1974) p. 9.

    Google Scholar 

  2. V. K. Zworykin, J. Hillier, and R. L. Snyder, ASTM Bull. 117, 15 (1942).

    Google Scholar 

  3. M. von Ardenne, Z. Phys., 109, 553 (1938).

    Article  Google Scholar 

  4. M. von Ardenne, Z. Techn. Phys., 19, 407 (1938).

    Google Scholar 

  5. D. McMullan, Ph.D. Dissertation, Cambridge University (1952).

    Google Scholar 

  6. K. C. A. Smith, Ph.D. Dissertation, Cambridge University (1956).

    Google Scholar 

  7. T. E. Everhart and R. F. M. Thornley, J. Sci. Instr., 37, 246 (1960).

    Article  Google Scholar 

  8. C. W. Oatley and T. E. Everhart, J. Electron., 2, 568 (1957).

    Google Scholar 

  9. R. F. W. Pease, Ph.D. Dissertation, Cambridge University (1963).

    Google Scholar 

  10. R. F. W. Pease and W. C. Nixon, J. Sci. Instr., 42, 81 (1965).

    Article  Google Scholar 

  11. A. V. Crewe, in Scanning Electron Microscopy/1974, IITRI, Chicago, Illinois (1969), p. 11.

    Google Scholar 

  12. D. G. Coates, Phil. Mag., 16, 1179 (1967).

    Article  CAS  Google Scholar 

  13. G. R. Booker, in Modern Diffraction Techniques in Materials Science (S. Amelincx, ed.), North Holland, Amsterdam (1970), p. 647.

    Google Scholar 

  14. J. R. Banbury, Ph.D. Dissertation, Cambridge University (1970).

    Google Scholar 

  15. D. C. Joy, Ph.D. Dissertation, Oxford University (1969).

    Google Scholar 

  16. J. Philibert and R. Tixier, Micron, 1, 174 (1969).

    Google Scholar 

  17. D. J. Fathers, J. P. Jakubovics, D. C. Joy, D. E. Newbury, and H. Yakowitz, phys. stat. sol. a, 20, 535 (1973).

    Article  Google Scholar 

  18. D. J. Fathers, J. P. Jakubovics, D. C. Joy, D. E. Newbury, and H. Yakowitz, phys. stat. sol. a 22, 609 (1974).

    Article  CAS  Google Scholar 

  19. K. F. J. Heinrich, C. E. Fiori, and H. Yakowitz, Science, 167, 1129 (1970).

    Article  CAS  Google Scholar 

  20. C. E. Fiori, H. Yakowitz, and D. E. Newbury, in Scanning Electron Microscopy/1974, IITRI, Chicago, Illinois (1974), p. 167.

    Google Scholar 

  21. C. J. D. Catto, Ph.D. Dissertation, Cambridge University (1972).

    Google Scholar 

  22. N. C. Yew and D. E. Pease, in Scanning Electron Microscopy/197b, IITRI, Chicago, Illinois (1974), p. 191.

    Google Scholar 

  23. J. Lebiedzik, K. G. Burke, S. Troutman, G. G. Johnson, Jr., and E. W. White, in Scanning Electron Microscopy/1974, IITRI, Chicago, Illinois (1974), p. 121.

    Google Scholar 

  24. R. F. Herzog, B. L. Lewis, and T. E. Everhart, in Scanning Electron Microscopy/ 1974, IITRI, Chicago, Illinois (1974), p. 175.

    Google Scholar 

  25. A. Boyde, in Scanning Electron Microscopy/1974, IITRI, Chicago, Illinois (1974), p. 91.

    Google Scholar 

  26. A. R. Dinnes, in Scanning Electron Microscopy: Systems and Applications 1973. Conference Series 18, Institute of Physics, London (1973), p. 76.

    Google Scholar 

  27. R. Fitzgerald, K. Keil, and K. F. J. Heinrich, Science, 159, 528 (1968).

    Article  CAS  Google Scholar 

  28. J. I. Goldstein and H. J. Axon, Naturwiss., 60, 313 (1973).

    Article  CAS  Google Scholar 

  29. K. F. J. Heinrich, in Fifty Years of Progress in Metallographic Techniques, ASTM Special Tech. Publ. No. 430 (1968), p. 315.

    Google Scholar 

  30. H. Moseley, Phil. Mag., 26, 1024 (1913).

    Google Scholar 

  31. J. Hillier, U.S. Pat. 2,418,029 (1947); L. L. Marton, U.S. Pat. 2,233,286 (1941).

    Google Scholar 

  32. R. Castaing and A. Guinier, in Proceedings of the 1st International Conference on Electron Microscopy, Delft, 1949, (1950), p. 60.

    Google Scholar 

  33. R. Castaing, Thesis, University of Paris (1951), ONERA publ. No. 55.

    Google Scholar 

  34. R. Castaing, in Advances in Electronics and Electron Physics Vol. 13 (1960), p. 317.

    Google Scholar 

  35. I. B. Borovskii and N. P. Ilin, Dokl Akad. Nauk SSSR, 106, 655 (1953).

    Google Scholar 

  36. M. E. Haine and T. Mulvey, J..Sci. Instr., 26, 350 (1959).

    Google Scholar 

  37. L. S. Birks and E. J. Brooks, Rev. Sci. Instr., 28, 709 (1957).

    Article  CAS  Google Scholar 

  38. R. M. Fisher and J. C. Schwarts, J. Appl. Phys., 28, 1377 (1957).

    Google Scholar 

  39. D. B. Wittry, Thesis, California Institute of Technology (1957).

    Google Scholar 

  40. J. R. Cuthill, L. L. Wyman, and H. Yakowitz, J. Metals, 15, 763 (1963).

    CAS  Google Scholar 

  41. V. E. Cosslett and P. Duncumb, Nature, 177, 1172 (1956).

    Article  Google Scholar 

  42. D. B. Wittry, in ASTM Spec. Techn. Publ. 349, (1963), p. 128.

    Google Scholar 

  43. J. Philibert, in X-Ray Optics and X-Ray Microanalysis (H. H. Pattee, V. E. Cosslett, and A. Engström, eds.), Academic Press, New York (1963), p. 379.

    Google Scholar 

  44. P. Duncumb and P. K. Shields, in The Electron Microprobe (T. D. McKinley, K. F. J. Heinrich, and D. B. Wittry, eds.), Wiley, New York (1966), p. 284.

    Google Scholar 

  45. B. L. Henke, in Advances in X-Ray Analysis, Vol. 7, Plenum Press, New York (1964), p. 460.

    Google Scholar 

  46. B. L. Henke, in Advances in X-Ray Analysis, Vol. 8, Plenum Press, New York (1965), p. 269.

    Google Scholar 

  47. J. V. P. Long and S. O. Agrell, Min. Mag., 34, 318 (1965).

    Article  CAS  Google Scholar 

  48. D. F. Kyser and D. B. Wittry, in The Electron Microprobe (T. D. McKinley, K. F. J. Heinrich, and D. B. Wittry, eds.), Wiley, New York, (1966), p. 691.

    Google Scholar 

  49. D. R. Beaman and J. A. Isasi, Anal. Chem., 42, 1540 (1970).

    Article  CAS  Google Scholar 

  50. H. Yakowitz, R. L. Myklebust, and K. F. J. Heinrich, Nat. Bureau of Standards Tech. Note 796 (1973).

    Google Scholar 

  51. N. C. Barbi, A. D. Sandborg, J. C. Russ, and C. E. Soderquist, in Scanning Electron Microscopy/1974, IITRI, Chicago, Illinois (1974), p. 151.

    Google Scholar 

Bibliography of Texts and Monographs in SEM and EPMA

  • 1951 R. Castaing, “Application of Electron Probes to Local Chemical and Crystallographic Analysis,” Ph. D. Thesis, University of Paris.

    Google Scholar 

  • 1966 H. A. Elion, Instrument and Chemical Analysis Aspects of Electron Microanalysis and Macroanalysis, Pergamon, New York.

    Google Scholar 

  • 1968 K. F. J. Heinrich (ed.), Quantitative Electron Probe Microanalysis, NBS Spec. Publ. 298.

    Google Scholar 

  • 1968 P. R. Thornton, Scanning Electron Microscopy, Chapman and Hall, London.

    Google Scholar 

  • 1969 A. J. Tousimis and L. L. Marton (eds.), Electron Probe Microanalysis, Advances in Electronics and Electron Physics (Suppl. 6), Academic Press, New York.

    Google Scholar 

  • 1971 L. S. Birks, Electron Probe Microanalysis, 2nd ed., Wiley-Interscience, New York.

    Google Scholar 

  • 1971 V. H. Heywood (ed.), Scanning Electron Microscopy—Systematic and Evolutionary Applications, Academic Press, London.

    Google Scholar 

  • 1972 D. R. Beaman and J. A. Isasi, Electron Beam Microanalysis, ASTM Spec. Tech. Publ. 506, 80 pp.

    Google Scholar 

  • 1972 J. W. S. Hearle, J. T. Sparrow, and P. M. Cross, The Use of the Scanning Electron Microscope, Pergamon Press, Oxford.

    Google Scholar 

  • 1972 C. W. Oatley, The Scanning Electron Microscope, University Press, Cambridge.

    Google Scholar 

  • 1973 C. A. Andersen (ed.), Microprobe Analysis, Wiley, New York.

    Google Scholar 

  • 1973 R. Woldseth, X-Ray Energy Spectrometry, Kevex, Burlingame, California.

    Google Scholar 

  • 1974 D. B. Holt, M. D. Muir, P. R. Grant, and I. M. Boswarva (eds.), Quantitative Scanning Electron Microscopy, Academic Press, London.

    Google Scholar 

  • 1974 O. C. Wells, Scanning Electron Microscopy, McGraw-Hill, New York.

    Google Scholar 

  • 1975 S. J. B. Reed, Electron Microprobe Analysis, University Press, Cambridge. The proceedings of the annual SEM conference sponsored by the Illinois Institute for Technology Research Institute (IITRI) each year since 1968 constitute the best source for individual research papers on SEM. Compiled and edited each year by Dr. O. Johari, this set of proceedings is necessary to any SEM laboratory. Current and past proceedings can be obtained from Dr. Johari at IITRI.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1975 Plenum Press, New York

About this chapter

Cite this chapter

Goldstein, J.I., Yakowitz, H., Newbury, D.E. (1975). Introduction. In: Goldstein, J.I., Yakowitz, H. (eds) Practical Scanning Electron Microscopy. Springer, Boston, MA. https://doi.org/10.1007/978-1-4613-4422-3_1

Download citation

  • DOI: https://doi.org/10.1007/978-1-4613-4422-3_1

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4613-4424-7

  • Online ISBN: 978-1-4613-4422-3

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics