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The effects of a spray slurry nozzle on copper CMP for reduction in slurry consumption

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Abstract

The environmental impact of semiconductor manufacturing has been a big social problem, like greenhouse gas emission. Chemical mechanical planarization (CMP), a wet process which consumes chemical slurries, seriously impacts environmental sustainability and cost-effectiveness. This paper demonstrates the superiority of a full-cone spray slurry nozzle to the conventional tube-type slurry nozzle in Cu CMP. It was observed that the spray nozzle made a weak slurry wave at the retaining ring unlike a conventional nozzle, because the slurry was supplied uniformly in broader areas. Experiments were implemented with different slurry flow rates and spray nozzle heights. Spray nozzle performance is controlled by the spray angle and spray height. The process temperature was obtained with an infrared (IR) sensor and an IR thermal imaging camera to investigate the cooling effect of the spray. The results show that the spray nozzle provides a higher Material removal rate (MRR), lower non-uniformity (NU), and lower temperature than the conventional nozzle. Computational fluid dynamics techniques show that the turbulence kinetic energy and slurry velocity of the spray nozzle are much higher than those of the conventional nozzle. Finally, it can be summarized that the spray nozzle plays a significant role in slurry efficiency by theory of Minimum quantity lubrication (MQL).

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References

  1. P. B. Zantye, A. Kumar and A. K. Sikdar, Chemical mechanical planarization for microelectronics applications, Material Science and Engineering, R 45 (2004) 89–220.

    Article  Google Scholar 

  2. G. C. C. Yang, CMP wastewater management using the concepts of design for environment, Environmental Progress, 21 (1) (2002).

    Google Scholar 

  3. P. Liu, X. C. Lu, Y. H. Liu, J. B. Luo and G. S. Pan, Chemical mechanical planarization of copper using ethylenediamine and hydrogen peroxide based slurry, Advanced Tribology (2010) 908–911.

    Google Scholar 

  4. D. H. Eom, I. K. Kim, J. H. Han and J. G. Park, The effect of hydrogen peroxide in a citric acid based copper slurry on Cu polishing, J. of Electrochemical Society, 154 (1) (2007) D38–D44.

    Article  Google Scholar 

  5. R. Ihnfeldt, Chemically impregnated abrasives provide high planarization efficiency copper CMP slurry, J. of Electrochemical Society, 61 (17) (2014) 1–13.

    Google Scholar 

  6. C. W. Wang, Y. L. Liu and J. Y. Tian, Planarization properties of an alkaline slurry without an inhibitor on copper patterned wafer CMP, J. of Semiconductors, 33 (11) (2012).

    Google Scholar 

  7. F. Testa, C. Coetsier, E. Carretier, M. Ennahali, B. Laborie and P. Moulin, Recycling a slurry for reuse in chemical mechanical planarization of tungsten wafer: Effect of chemical adjustments and comparison between static and dynamic experiments, Microelectronic Engineering, 113 (2014) 114–122.

    Article  Google Scholar 

  8. B. Horacek, K. T. Kiger and J. H. Kim, Single nozzle spray cooling heat transfer mechanisms, Int. J. of Heat and Mass Transfer, 48 (2005) 1425–1438.

    Article  Google Scholar 

  9. S. Shiva Sai, K. Manoj Kumar and A. Ghosh, Assessment of spray quality from an external mix nozzle and its impact on SQL grinding performance, Int. J. of Machine Tools & Manufacture, 89 (2015) 132–141.

    Article  Google Scholar 

  10. H. S. Lee, Y. B. Park and S. J Lee, Preliminary study on the effect of spray slurry nozzle in CMP for environmental sustainability, Int. J. Precision Manufacturing, 15 (6) (2014) 995–1000.

    Article  Google Scholar 

  11. H. S. Lee, Y. B. Park and H. D Jeong, Influence of slurry components on uniformity in copper chemical mechanical planarization, Microelectronic Engineering, 85 (2008) 689–696.

    Article  Google Scholar 

  12. A. Philipossian, L. Borucki, Y. Sampurno and Y. Zhuang, Novel slurry injection system for improved slurry flow and reduced defects in CMP, Proceedings of the UCPSS (2014).

    Google Scholar 

  13. D. Wang, J. Lee, K. Holland, T. Bibby, S. Beaudoin and T. Cale, Von mises stress in chemical-mechanical polishing processes, J. of Electrochemical Society, 144 (1997).

  14. Y. Y. Zhou and E. C. Davis, Variation of polish pad shape during pad dressing, Material Science and Engineering, B 68 (1999).

  15. J. Sorooshian, D. DeNardis, L. Charns, Z. Li, F. Shadman, D. Boning, D. Hetherington and A. Philipossiana, Arrehenius characterization of ILD and copper CMP processes, J. of The Electrochemical Society, 151 (2) (2004) G85–G88.

    Article  Google Scholar 

  16. F. P. Karrholm, Numerical modelling of diesel spray infection, turbuleca interaction and combustion, Thesis for the degree of doctor of philosophy in Thermo and Fluid Dynamics (2008).

    Google Scholar 

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Correspondence to Haedo Jeong.

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Recommended by Guest Editor Sangho Park

Dasol Lee is a M.S student of School of Mechanical Engineering, Pusan National University, Busan, Korea. She received her B.S. degree in Materials Science and Engineering from Pusan National University. Her research interests include chemical mechanical polishing of electronic materials and manufacturing.

Haedo Jeong is a professor at the School of Mechanical Engineering, Pusan National University, Busan, Korea. He received his B.S. and M.S. degrees from Pusan National University and Korea Advanced Institute of Science and Technology (KAIST), respectively. Then, he received his Ph.D. degree in Mechanical Engineering from Tokyo University, Japan in 1994. His research fields include chemical mechanical polishing (CMP), grinding, polisher and consumable design, and post-CMP cleaning.

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Lee, D., Lee, H. & Jeong, H. The effects of a spray slurry nozzle on copper CMP for reduction in slurry consumption. J Mech Sci Technol 29, 5057–5062 (2015). https://doi.org/10.1007/s12206-015-1101-2

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  • DOI: https://doi.org/10.1007/s12206-015-1101-2

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