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Sonochemical Synthesis, Characterization and Sonocatalytic Performance of Terbium-Doped CdS Nanoparticles

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Abstract

Terbium-doped cadmium sulfide nanoparticles with different terbium contents were successfully synthesized via sonochemical route. The prepared samples were characterized by X-ray diffraction, scanning electron microscopy, photoelectron X-ray spectroscopy, and UV–Vis diffuse reflectance spectroscopy techniques. The as-prepared nanocatalyst were used for sonocatalytic degradation of Methylene Blue. Among the different amounts of dopant, 8 % Tb-doped CdS showed the highest sonocatalytic activity. The order of inhibitory effect of radical scavengers was 1, 4 Benzoquinone > SO3 2− > CO2 3−> I. The effects of various parameters such as initial dye concentration, catalyst loading, ultrasonic power, and the presence of radical scavengers were investigated.

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Acknowledgments

This work is funded by the Grant NRF-2015-002423 of the National Research Foundation of Korea.

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Correspondence to Younes Hanifehpour, Babak Mirtamizdoust or Sang Woo Joo.

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Hanifehpour, Y., Hamnabard, N., Mirtamizdoust, B. et al. Sonochemical Synthesis, Characterization and Sonocatalytic Performance of Terbium-Doped CdS Nanoparticles. J Inorg Organomet Polym 26, 623–631 (2016). https://doi.org/10.1007/s10904-016-0352-4

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  • DOI: https://doi.org/10.1007/s10904-016-0352-4

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