Optimization of Process Parameters of Zirconia Reinforced Alumina by Powder Forming Process Using Response Surface Method

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Abstract:

Powder forming process is used for fabrication of bulk ceramic components. Optimization of powder forming process parameters in the fabrication of alumina-zirconia composite used in orthopedic implants is done for desired physical property. In this research work, process parameters such as composition of zirconia, compaction pressure and sintering temperature were analyzed using Response Surface Method (RSM). The physical properties such as density, porosity and water absorption characteristics of the proposed composite were studied. To study the influence of the different process parameters over the physical properties of the fabricated composites materials, experimental runs were framed by using Box behnken method. Three factors and two levels were selected with a total of 17 runs and their consecutive tests were carried out. The validity of the model was checked and the significant parameters were identified using Analysis of variance (ANOVA). The results indicate that the sintering temperature is influencing predominantly the physical properties of composites compared to other process parameters.

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Periodical:

Advanced Materials Research (Volumes 984-985)

Pages:

129-139

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Online since:

July 2014

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[1] Crack growth resistance of alumina, zirconia and zirconia toughened alumina ceramics for joint prostheses. A.H. DeAza, J. Chevalier, G. Fantozzi, M. Schehl, R. Torrecillas, Biomaterials 23(2002)937–945.

DOI: 10.1016/s0142-9612(01)00206-x

Google Scholar

[2] LawnB. Fracture of brittle solids. Cambridge solid state science series 2nded. UK: Cam bridge university press, 1993, p.378.

Google Scholar

[3] Willmann G. Ceramic femoral heads for total hip arthroplasty. Advanced Eng Mater2000; 2: 114–22.

Google Scholar

[4] HerosR, WillmannG. Ceramics in total hip arthroplasty: history, mechanical properties, clinical results and current manufacturing state of the art. Seminars Arthroplasty 1998; 9: 114–22.

Google Scholar

[5] PiconiC, MaccauroG. Zirconia as a ceramic biomaterial, a review. Biomaterials 1999; 20: 1–25.

Google Scholar

[6] HanninkRH, KellyPM, MuddleBC. Transformation toughening in zirconia containing ceramics. J Am Ceram Soc 2000; 83(3): 461–87.

Google Scholar

[7] Kelly P M, Francis Rose L R. The martensitic transformation in ceramics its role in transformation toughening. Prog Mater Sci2002; 47: 463–557.

DOI: 10.1016/s0079-6425(00)00005-0

Google Scholar

[8] Hannink R H J, Kelly P M, Muddle B C. Transformation toughening in zirconia containing ceramics. J Am Ceram Soc 2000; 83: 461 –87.

DOI: 10.1111/j.1151-2916.2000.tb01221.x

Google Scholar

[9] DrouinJM, CalesB. Yttria-stabilized zirconia for improved hip joint head. In: Andersson . O OH, Yli UrpoA, editors. Bioceramics7. London: Butterworth F Heinemann Publisher, 1994. P . 387–94.

Google Scholar

[10] ChevalierJ, Drouin J M, Cales B. Low temperature ageing behavior of zirconia hip joint heads. In: Sedel L, ReyC, editors. Bioceramics, Proceedings of the10th International Symposiumon Ceramics in Medicine, vol. 10. Amsterdam: ElsevierLtd., 1997. p.135.

DOI: 10.1016/b978-008042692-1/50032-7

Google Scholar

[11] ChevalierJ, CalesB, DrouinJM. Low temperature aging of YTZP ceramics. J Am Ceram Soc 1999; 82 (8): 2150–4.

Google Scholar

[12] Chevalier J, DeAza A H, FantozziG , Scheh l M, Torrecillas R. Extending the life time of orthopaedic implants. Advanced Mater 2000; 12(21): 1619–21.

Google Scholar

[13] Montgomerry D.C. 2001. Design and Analysis of Experiments,. 5th ed., John Wiley Sons, New York, USA.

Google Scholar

[14] Preliminary Biocompatibility and Bioactivity Properties of Alumina-Zirconia-Hydroxyapatite Composite, Rodica Rogojan, Ecaterina Andronescu, Maria Cristina Munteanu, Mihaela Radu, Florina Gisela Gaina, Roxana Trusca.

Google Scholar