Flexible Electrochemical Platform Coupled with In Situ Prepared Synthetic Receptors for Sensitive Detection of Bisphenol A
Abstract
:1. Introduction
2. Experimental
2.1. Reagents and Apparatus
2.2. Preparation of MIP or NIP Modified Electrodes
2.3. Bisphenol A Electrochemical Measurement
2.4. Real Sample Analysis
3. Results and Discussions
3.1. Characterization of CF, Bisphenol A–MIP@CF, MIP@CF
3.2. Flexibility Tests of MIP@CF
3.3. Electrochemical Behaviors of Different Modified Electrodes
3.4. Parameters Optimization for Sensor Preparation
3.5. Sensing-Performance of MIP@CF in Bisphenol A Detection
3.6. Selectivity
3.7. Reproducibility and Stability of the Sensor
3.8. Real Samples Analysis
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
Abbreviations
References
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Electrode | Method | Linear Range (μM) | LOD (nM) | Reference |
---|---|---|---|---|
MWCNTs-βCD/SPCE | LSV | 0.125–2/2–30 | 13.7 | [50] |
CTAB/MIL-101(Cr) | DPV | 0.02–0.35 | 10 | [51] |
NiFe2O4/SPCE | DPV | 0.02–12.5 | 6 | [52] |
AgNPs-EG | SWV | 5–100 | 230 | [19] |
AuNDs@CNFs/SPE | DPV | 0.01–50 | 5 | [53] |
GO-MWCNT-βCD/SPE | LSV | 0.05–5/5–30 | 6 | [43] |
BZPY/MCPE | DPV | 2–18 | 29 | [54] |
MIP@CF | DPV | 0.0005–0.008/0.01–0.3 | 0.36 | This work |
Sample | Original (nM) | Added (nM) | Found (nM) | Recovery (%) | RSD (%) |
---|---|---|---|---|---|
Milk | 0.00 | 1.00 | 1.12 | 112 | 3.96 |
0.00 | 50.00 | 51.28 | 102.5 | 4.16 | |
0.00 | 200.00 | 182.50 | 91.26 | 3.54 |
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Xu, C.-Y.; Ning, K.-P.; Wang, Z.; Yao, Y.; Xu, Q.; Hu, X.-Y. Flexible Electrochemical Platform Coupled with In Situ Prepared Synthetic Receptors for Sensitive Detection of Bisphenol A. Biosensors 2022, 12, 1076. https://doi.org/10.3390/bios12121076
Xu C-Y, Ning K-P, Wang Z, Yao Y, Xu Q, Hu X-Y. Flexible Electrochemical Platform Coupled with In Situ Prepared Synthetic Receptors for Sensitive Detection of Bisphenol A. Biosensors. 2022; 12(12):1076. https://doi.org/10.3390/bios12121076
Chicago/Turabian StyleXu, Chen-Yan, Kang-Ping Ning, Zheng Wang, Yao Yao, Qin Xu, and Xiao-Ya Hu. 2022. "Flexible Electrochemical Platform Coupled with In Situ Prepared Synthetic Receptors for Sensitive Detection of Bisphenol A" Biosensors 12, no. 12: 1076. https://doi.org/10.3390/bios12121076