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High Temperature X-Ray Diffraction in Transmission Under Controlled Environment

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Abstract

A compact tube furnace has been developed for high temperature X-ray diffraction studies using high energy synchrotron radiation. The furnace design has a low absorption path in transmission yet allows for a high degree of control of the sample atmosphere and a minimal temperature gradient across the sample. The design allows for a maximum temperature of 1500°C with a variety of atmospheres including inert, reducing, and oxidizing. Preliminary results obtained at the SRI-CAT I-ID undulator line (60keV) at the APS facility and the A2 24 pole wiggler line (45keV) at CHESS on the Ti5Si3Z5 (Z = C, N, O) system will be presented to demonstrate the feasibility of this approach.

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Authors and Affiliations

  1. Ames Laboratory, Iowa State University, Ames, IA, 50011, USA

    L. Margulies, M. J. Kramer, J. J. Williams, E. M. Deters, R. W. McCallum & A. I. Goldman

  2. APS, Argonne National Laboratory, Argonne, Il, 60439, USA

    D. R. Haeffner & J. C. Lang

  3. CHESS, Cornell University, Ithaca, NY, 14853, USA

    S. Kycia

Authors
  1. L. Margulies
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  2. M. J. Kramer
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  3. J. J. Williams
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  4. E. M. Deters
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  5. R. W. McCallum
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  6. D. R. Haeffner
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  7. J. C. Lang
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  8. S. Kycia
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  9. A. I. Goldman
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Correspondence to L. Margulies.

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Margulies, L., Kramer, M.J., Williams, J.J. et al. High Temperature X-Ray Diffraction in Transmission Under Controlled Environment. MRS Online Proceedings Library 524, 139–144 (1998). https://doi.org/10.1557/PROC-524-139

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  • DOI: https://doi.org/10.1557/PROC-524-139

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