RDF method application to phase analysis of X-ray amorphous products of gibbsite thermal activation

K.I. Shefer; E.M. Moroz; L.I. Isupova; I.V. Kharina; Yu.Yu. Tanashev

Publicly Available Published by Oldenbourg Wissenschaftsverlag 2007

RDF method application to phase analysis of X-ray amorphous products of gibbsite thermal activation

From the book Tenth European Powder Diffraction Conference

K.I. Shefer , E.M. Moroz , L.I. Isupova , I.V. Kharina and Yu.Yu. Tanashev

https://doi.org/10.1524/9783486992540-044

From the book

$Tenth European Powder Diffraction Conference$

Tenth European Powder Diffraction Conference

Chapters in this book (99)

Frontmatter

Preface

Editorial Notes

European Powder Diffraction Conference Award

Table of Contents

Powder diffraction studies on proteins: An overview of data collection approaches

I. METHOD DEVELOPMENT AND APPLICATION

I.1 Determination of Crystal Structure

Nanostructure studied using the atomic pair distribution function

Likelihood methods with protein powder diffraction data

The complementary use of solid state NMR and XRD to solve zeolite structures

Exploiting X-ray induced anisotropic lattice changes to improve intensity extraction in protein powder diffraction: Application to heavy atom detection

Aspects of validation in the structure determination of organic materials from powder X-ray diffraction data

Validation of magnetic structures

I.2 Qualitative and Quantitative Phase Analysis

New horizons for the structural characterization of stainless steel slags by X-ray powder diffraction

Method for quick estimation of the Sb³⁺/Sb⁵⁺ content ratio in ATO

Evaluation of the phase detection limit on filter-deposited dust particles from Antarctic ice cores

I.3 Analysis of Microstructure and Macrostress

I.3.1 Residual Stresses

In-situ investigation by X-ray diffraction and wafer curvature of phase formation and stress evolution during metal thin film – silicon reactions

Residual stress profile in ceramic laminates

I.3.2 Line Broadening Analysis

Powder diffraction characterization of stacking disorder

A Debye function based powder diffraction data analysis method

Illite crystallinity: Instrumental effect and its relation to crystallite size and lattice distortion

Size-related diffraction anomalies from strongly distorted nano-crystals

I.4 Texture

Rietveld texture analysis from diffraction images

Secondary extinction correction used in a novel method for improved XRD characterizations of textured materials: The case of thin films

II. INSTRUMENTAL

In-situ powder diffraction in high magnetic fields

Characterization of a high performance laboratory parallel-beam diffractometer – bridging the gap to the synchrotron

Design of powder diffraction beamline (BL-I11) at Diamond

In-situ analysis of crystallographic texture using high-energy X-rays

Installation of the high resolution TOF diffractometer at the Budapest Research Reactor

Stress and local texture measurements at the materials science diffractometer STRESS-SPEC at FRM-II

Versatile IBARAKI materials design neutron diffractometer at J-PARC

From powder diffraction to structure resolution of nanocrystals by precession electron diffraction

III. SOFTWARE

Powder pattern indexing and the dichotomy algorithm

EFLECH/INDEX – Another try of whole pattern indexing

Predicted corner-sharing titanium silicates

Using the Cambridge Structural Database to validate powder structures

Two-dimensional powder diffraction

IV. MATERIALS

IV.1 Thin Layers

X-ray diffraction analysis of an ε/γʹ – ironnitride compound double layer

Texture of submicron Ni-Mn-Ga films studied by X-ray diffraction at the ANKA synchrotron source

Texture and stress in nickel layers with incorporated zirconia particles

Growth of magnetron sputtered TiO₂ thin films studied by X-ray scattering

Study of crystallization of magnetron sputtered TiO₂ thin films by X-ray scattering

IV.2 Nanocrystalline and Amorphous Materials

Transition of nc-SiC powder surface into grain boundaries during sintering by molecular dynamics simulation and neutron powder diffraction

Evolution of the microstructure in nanocrystalline copper electrodeposits during room temperature storage

Melting of small silver clusters investigated by HT-GIXRD

The use of RDF analysis in the study of powder samples: Zirconia complex supported by clay and pseudoboehmite

RDF method application to phase analysis of X-ray amorphous products of gibbsite thermal activation

Study of nanoalloys formation mechanism from single-source precursors [M(NH₃)₅Cl](ReO₄)₂, M = Rh, Ir

Synthesis and thermal decomposition of the oxalatho cuprates(II) – [M(NH₃)₄][Cu(C₂O₄)₂]*3H₂O, M = Pt, Pd

IV.3 Metals and Alloys

IV.3.1 General

HT-XRD in the study of Cu-Li-Mg

Phase distribution of friction welded Ti6Al4V/γ-TAB

Mixed site occupancies in μ-Zr-Nb-Al by resonant powder diffraction

Gold leaf decoration on medieval islamic glazed ceramics – in search of technological features with XRD

IV.3.2 Microstructure, Stress and Texture

Use of generalised pole figures in the X-ray study of textured metal materials

Reconstruction of high-temperature deformation process by texture of the low-temperature phase as applied to Zrbased alloys

X-ray studies of nanostructured metals processed by severe plastic deformation

Microstructure evolution of nanocrystalline HITPERM and NANOPERM alloys: Insight from in-situ synchrotron radiation experiments

Time resolved in-situ synchrotron radiation diffraction investigation of grain-growth kinetics in magnetic nanocomposites

Triaxial residual stresses in composite tube from austenitic stainless steel with welded ferritic steel cladding

Neutron diffraction investigation of the residual stress gradient near stainless steel – zirconium alloy interface

IV.4 Minerals and Inorganics

IV.4.1 Structural Changes, In-situ and Non-Ambient Investigations

High temperature X-ray diffraction investigation of an aluminium-siliconcorundum system

Investigation of the βʹ to α-phase transformation temperature of (Ca_1-xMg_x)₃(PO₄)₂ solid solutions

Vacancies ordering in La³⁺_1-xBa²⁺_xFeO_3-δ perovskites

In-situ investigations of LiMn₂O₄ at high pressure

Structural study of pure silica and Gecontaining zeolite ITQ-24

Structure properties of chemisorbed methyl groups in the framework of faujasite zeolitic catalysts

Synchrotron radiation XRPD study on the early hydration of cements

Effect of interlayer cation and relative humidity on the hydration properties of a dioctahedral smectite

Time-resolved synchrotron X-ray powder diffraction study of biogenic nanomagnetite

Utilizing total scattering to study the Jahn-Teller transition in La_1-xCa_xMnO₃

Neutron diffraction study of Pr_0.5Ca_0.5CoO_3-γ (γ=0 and 0.07)

Advances in the characterisation of domain switching in ferroelectric ceramics

The nature of special points on unit cell parameters temperature dependences for crystal substances

IV.4.2 Determination of Crystal Structure; Structure Refinement

Combined high resolution powder and single-crystal diffraction to determine the structure of Li^1+xCe^III_xCe^IV_6-xF₂₅

Crystal Structure of the Ba₃MgSi₂O₈:Mn²⁺,Eu²⁺ phosphor for white light emitting diodes

Rietveld refinements of SnO₂ ceramic powders doped with ZnO, WO₃, CoO, Nb₂O₅ and MoO₃

Synchrotron X-ray powder diffraction studies of solubility limits in the LiFe₅O₈-LiAl₅O₈ spinel solid solutions

Synchrotron X-ray diffraction study on the cation distribution in quaternary Li-Fe-Mn spinel oxides

Diffraction analysis of the lithium battery cathode material Li_1.2Mn_0.4Ni_0.3Co_0.1O₂

Defect structure examination of Sn-doped indium oxide (ITO)

Modulation of Cu-O chain length in SmBa₂Cu₃O_6+δ, by Al doping and clustering

Simulation of the XRD patterns, structural properties of a synthetic Na-Hectorite exchanged Cu²⁺ and Ca²⁺

IV.4.3 Determination of Magnetic Structure, Magnetic Materials

Intermediate phase in the oxidative hydrothermal synthesis of potassium jarosite, a model kagomé antiferromagnet

Neutron powder diffraction study on the magnetic ordering and structure of Li_xMn_3-x-yFe_yO₄ spinels

IV.4.4 Microstructure, Phase Analysis

Phase composition and thermal expansion behaviour of zirconium tungstate prepared by rapid sintering

X-ray phase analysis in leucite systems

Structural analysis by the Rietveld method and SEM of irradiated pseudoboehmite and Al₂O₃

Rietveld refinement of ZrSiO₄: Application of a phenomenological model of anisotropic peak width

X-ray diffraction line broadening in dry grinding of kaolinite

IV.5 Organic Materials

Microstructure of energetic crystals – grain by grain via rocking curve

The presence of polymorphism in oxytetracycline hydrochloride shown by X-ray powder diffraction techniques

Synthesis and structural characterization of mixed transition metal derivatives of maleic acid: (M²⁺_0.5Fe²⁺_0.5)(C₄H₃O₄)^-₂·4H₂O (with M²⁺=Mn, Co, Ni, and Zn) using powder diffraction data

Structure determination and phase transition behaviour of mesitylene

Structures of transition metal hydroxyterephthalates

Analysis of intra- and intermolecular hydrogen bonding in androstane derivatives: A case study of steroids

Structures of magnesium and zinc long aliphatic chains carboxylates

The crystal structures of the β1 and β2 polymorphs of mono-unsaturated triacylglycerols and cocoa butter determined from high resolution powder diffraction data

Microphase separation in semifluorinated polyesters

Powder diffraction studies of organoammonium polymolibdates

Author Index