王雪媛, 高琨, 陈芹芹, 毕金峰, 吴昕烨, 易建勇. 苹果片中短波红外干燥过程中水分扩散特性[J]. 农业工程学报, 2015, 31(12): 275-281. DOI: 10.11975/j.issn.1002-6819.2015.12.037
    引用本文: 王雪媛, 高琨, 陈芹芹, 毕金峰, 吴昕烨, 易建勇. 苹果片中短波红外干燥过程中水分扩散特性[J]. 农业工程学报, 2015, 31(12): 275-281. DOI: 10.11975/j.issn.1002-6819.2015.12.037
    Wang Xueyuan, Gao Kun, Chen Qinqin, Bi Jinfeng, Wu Xinye, Yi Jianyong. Water diffusion characteristics of apple slices during short and medium-wave infrared drying[J]. Transactions of the Chinese Society of Agricultural Engineering (Transactions of the CSAE), 2015, 31(12): 275-281. DOI: 10.11975/j.issn.1002-6819.2015.12.037
    Citation: Wang Xueyuan, Gao Kun, Chen Qinqin, Bi Jinfeng, Wu Xinye, Yi Jianyong. Water diffusion characteristics of apple slices during short and medium-wave infrared drying[J]. Transactions of the Chinese Society of Agricultural Engineering (Transactions of the CSAE), 2015, 31(12): 275-281. DOI: 10.11975/j.issn.1002-6819.2015.12.037

    苹果片中短波红外干燥过程中水分扩散特性

    Water diffusion characteristics of apple slices during short and medium-wave infrared drying

    • 摘要: 为了研究苹果片中短波干燥过程中水分扩散特性和玻璃化转变温度的变化规律,进而明确中短波红外干燥过程中的水分扩散特性,采用中短波红外干燥箱在50、70和90℃的条件下对苹果片进行中短波红外干燥处理试验,应用低场核磁共振(low-field nuclear resonance,LF-NMR)和差示量热扫描(differential scanning calorimetry,DSC)等技术,测定中短波红外干燥过程中水分状态、玻璃化转变温度、水分活度、体积等变化情况,进一步分析中短波红外干燥过程中水分状态与玻璃化转变温度、水分活度等指标之间的相关性及变化规律。结果表明:干燥过程中,中短波红外温度对水分扩散影响较大,50、70、90℃3个温度条件下平均干燥速率之比为1∶1.5∶2.3;苹果片中存在3种状态水分,干燥过程中液泡中的自由水含量大幅度降低的同时,细胞质和细胞外空隙中不易流动水质量分数由7.96%增加至46.82%,干燥继续进行,不易流动水含量逐渐降低;中短波红外干燥过程中,苹果片内不易流动水含量的降低,明显提高了玻璃化转变温度(p<0.05),使其由?38℃左右最高上升至13.41℃,并引起水分活度由0.99迅速下降至0.24(p<0.01);随干燥过程中水分的散失,苹果片发生皱缩现象,体积与水分含量表现出极显著相关性(R>0.99)。该研究为中短波红外干燥中水分扩散特性研究提供了理论依据。

       

      Abstract: Abstract: Drying is an effective method for the food industry to extend product's shelf life, which makes the moisture content of the food reduce to a certain extent to ensure microbial stability of the product. Compared to traditional air drying method, short and medium wave infrared drying takes shorter time to evaporate moisture. Water plays a critical role in the chemical and enzymatic reactions and alters material properties. Moisture transfer is therefore a governing factor in drying process. However, heat and moisture transfer in fruits and vegetables drying is a complex process. A better understanding of the mechanism of moisture transfer will be helpful to improve product quality and the efficiency of drying process. In order to investigate the changing rules of water characteristics and glass transition temperature in apple slices during short and medium wave infrared drying, low-field nuclear magnetic resonance (LF-NMR), differential scanning calorimetry (DSC) and other instruments were applied in the test. LF-NMR is commonly used to detect changes in water status with the advantages of fast and non-destructive analysis. It can explain the migration of water from microscopic point of view through its relaxation behavior of inner protons. Results showed that short and medium wave infrared temperatures had strong influence on water diffusion, and the ratio of average drying rates under 50, 70 and 90 ℃ was 1:1.5:2.3. Three kind of water states were obtained from the LF-NMR experiments using the Carr-Purcell-Meiboom-Gill (CPMG) pulse sequences, and among the transverse relaxation time (T2), T21 (1-20 ms), T22 (20-200 ms) and T23 (200-1 000 ms) were corresponding to bound water, immobilized water and free water respectively, which implied that the longer the relaxation time, the stronger the water flow. The dramatically decreased content of free water content in vacuoles was accompanied by the sharp increase in the content of immobilized water in the cytoplasm and extra-cellular space, from 7.96% to 46.82%. Subsequently, the content of immobilized water decreased gradually with time increasing. Short and medium wave infrared drying elevated the glass transition temperature (P<0.05) and reduced water activity (P<0.01) appreciably by decreasing the content of immobilized water in apple tissues, which showed high correlation between glass transition temperature or water activity and water status. Obviously shrinkage occurred in apple slices along with the water loss in the process of drying, and volume and moisture content showed a significant correlation (R>0.99). This research provides the theoretical basis for understanding the water diffusion characteristics of short and medium wave infrared drying.

       

    /

    返回文章
    返回