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Programming of temperature and flow rate of carrier gas in work with polycapillary columns for gas-liquid chromatography

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Abstract

Methods of programming temperature and flow rate of carrier gas for to reducing the time of analyte separation on polycapillary columns (PCC) are compared. As was shown, the programming of temperature is accompanied by a change of peak shape, associated with the irregular heating of PCC capillaries. The programming of carrier gas flow rate does not distort the shape of chromatography peaks and does not require long time to return the system to the starting conditions.

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Authors and Affiliations

  1. Faculty of Physical Sciences, Novosibirsk State University, ul. Pirogova 2, Novosibirsk, 630090, Russia

    O. A. Nikolaeva, Yu. V. Patrushev & V. N. Sidel’nikov

  2. Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, pr. Akad. Lavrent’eva 5, Novosibirsk, 630090, Russia

    O. A. Nikolaeva & Yu. V. Patrushev

Authors
  1. O. A. Nikolaeva
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  2. Yu. V. Patrushev
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  3. V. N. Sidel’nikov
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Correspondence to O. A. Nikolaeva.

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Original Russian Text © O.A. Nikolaeva, Yu.V. Patrushev, V.N. Sidel’nikov, 2014, published in Zhurnal Analiticheskoi Khimii, 2014, Vol. 69, No. 6, pp. 621–625.

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Nikolaeva, O.A., Patrushev, Y.V. & Sidel’nikov, V.N. Programming of temperature and flow rate of carrier gas in work with polycapillary columns for gas-liquid chromatography. J Anal Chem 69, 559–562 (2014). https://doi.org/10.1134/S1061934814060124

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  • DOI: https://doi.org/10.1134/S1061934814060124

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