Issue 9, 1981
From the journal:

Journal of the Chemical Society, Dalton Transactions

Notes. Crystal structure of biphenyl-2,2′-diyltriphenylantimony

Peter L. Millington  and  D. Bryan Sowerby  

Abstract

An X-ray analysis of the title compound shows slightly distorted trigonal-bipyramidal geometry about the central atom in contrast to the square-pyramidal co-ordination in the related SbPh5. The heavy-atom method was used with X-ray diffractometer data and refinement by full-matrix least squares converged at R 0.036 for 3 367 reflections. Crystals are monoclinic, space group P21/n, with a= 10.488(5), b= 16.561(8), c= 13.503(6)Å, β= 92.16(2)°, and Z= 4.

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Article information

DOI
https://doi.org/10.1039/DT9810002011
Article type
Paper

J. Chem. Soc., Dalton Trans., 1981, 2011-2013

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Notes. Crystal structure of biphenyl-2,2′-diyltriphenylantimony

P. L. Millington and D. B. Sowerby, J. Chem. Soc., Dalton Trans., 1981, 2011 DOI: 10.1039/DT9810002011

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