A solvent-free route is developed for synthesizing titanosilicate zeolites with good crystallinity, uniform crystals, high surface area, and tetrahedral Ti species in the framework. Catalytic tests show that S-TS-1 exhibits almost the same catalytic activity in hexane oxidation with H2O2 as that of conventional TS-1 synthesized by a hydrothermal route.
L. Zhu, J. Zhang, L. Wang, Q. Wu, C. Bian, S. Pan, X. Meng and F. Xiao, J. Mater. Chem. A, 2015, 3, 14093 DOI: 10.1039/C5TA02680F
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