Macrocycles containing two o-iminoanilino units undergo stereoselective C-alkylation on treatment with Grignard reagents or lithium alkyls to give the meso-dialkyl-substituted macrocyclic tetra-amines.
K. Henrick, P. M. Judd, P. G. Owston, R. Peters, P. A. Tasker and R. W. Turner, J. Chem. Soc., Chem. Commun., 1983, 1253 DOI: 10.1039/C39830001253
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