Methods for synthesis of cluster complexes containing triangular arrangements of metal atoms capped by alkylidyne ligands are reported, and such structures confirmed by X-ray diffraction studies on the compounds [FePtW(µ3-CC6H4Me-4)(CO)6(PEt3)(η-C5H5)] and [FeRhW(µ3-CC6H4Me-4)(µ2-CO)(CO)5(η-C5H5)(η-C9H7)].
M. Chetcuti, M. Green, J. A. K. Howard, J. C. Jeffery, R. M. Mills, G. N. Pain, S. J. Porter, F. G. A. Stone, A. A. Wilson and P. Woodward, J. Chem. Soc., Chem. Commun., 1980, 1057 DOI: 10.1039/C39800001057
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