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The unique trigonal bipyramidal Pb52– and unicapped antiprismatic Sn94– anions have been discovered by X-ray structural studies on their salts with Na+(2,2,2-crypt).
J. D. Corbett and P. A. Edwards, J. Chem. Soc., Chem. Commun., 1975, 984 DOI: 10.1039/C39750000984
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