Low temperature 1H and 11B n.m.r. spectra of B6H10 and 2-MeB6H9 demonstrate: (1) the bridge proton exchange rate is slow on the n.m.r. time scale; (2) the spectra of B6H10 thus obtained are consistent with the known solid state structure; and (3) the static structure of 2-MeB6H9 is without a mirror plane of symmetry.
V. T. Brice, H. D. Johnson and S. G. Shore, J. Chem. Soc., Chem. Commun., 1972, 1128 DOI: 10.1039/C39720001128
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