Synthesis of LiyMnSiOx and LiMnPO4nanostructures

Bettina Milke; Peter Strauch; Markus Antonietti; Cristina Giordano

doi:10.1039/B9NR00149B

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Synthesis of Li_yMnSiO_x and LiMnPO₄nanostructures†

Bettina Milke,^a Peter Strauch,^a Markus Antonietti^a and Cristina Giordano*^a

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* Corresponding authors

^a Max-Planck-Institute of Colloids and Interfaces, Colloid Chemistry Research Campus Golm, Am Muehlenberg, Golm, Germany

Abstract

Nanosized Li_yMnSiO_x and LiMnPO₄ have been synthesized by a hydrothermal route. Simply by changing parameters such as metal precursors and/or template, high surface area Li_yMnSiO_x with different morphology and sizes were prepared, in particular hollow spheres and plate-like nanoparticles, however with poorly developed crystallinity. In the case of LiMnPO₄, highly crystalline nanocrystals were prepared.

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Supplementary files

FT-IR spectra of Li_yMnSiO_x prepared with different silica sources and differentmetal precursors; particles size distributions of Li_yMnSiO_x in the form of hollow spheres and plate-likenanoparticles; ICP technical details PDF (171K)

Article information

DOI: https://doi.org/10.1039/B9NR00149B
Article type: Communication
Submitted: 23 Jun 2009
Accepted: 10 Aug 2009
First published: 28 Aug 2009

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Nanoscale, 2009,1, 110-113

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Synthesis of Li_yMnSiO_x and LiMnPO₄nanostructures

B. Milke, P. Strauch, M. Antonietti and C. Giordano, Nanoscale, 2009, 1, 110 DOI: 10.1039/B9NR00149B

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