Issue 4, 2001
From the journal:

Chemical Communications

A highly efficient synthetic procedure for deuteriating imidazoles and imidazolium salts

Christopher Hardacre,*a   John D. Holbreyb  and  S. E. Jane McMatha  

* Corresponding authors

a School of Chemistry, The Queen’s University of Belfast, Belfast, Northern Ireland

b The QUILL centre, The Queen’s University of Belfast, Belfast, Northern Ireland.
E-mail: c.hardacre@qub.ac.uk;
Fax: +44 28 9038 2117;
Tel: +44 28 9027 4592

Abstract

Both substituted imidazoles and 1,3-dialkylimidazolium salts can be fully deuteriated on the heterocyclic ring using D2O over heterogeneous Pd catalysts: deuteriated 1-alkyl-3-methylimidazolium chloride and hexafluorophosphate ionic liquids can also be prepared in good yields utilising readily available and relatively low cost sources of deuterium.

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Article information

DOI
https://doi.org/10.1039/B009097M
Article type
Communication
Submitted
13 Nov 2000
Accepted
17 Jan 2001
First published
08 Feb 2001

Chem. Commun., 2001, 367-368

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A highly efficient synthetic procedure for deuteriating

imidazoles and imidazolium salts

C. Hardacre, J. D. Holbrey and S. E. J. McMath, Chem. Commun., 2001, 367 DOI: 10.1039/B009097M

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