A new layered mixed metal methylphosphonate, which contains interlayer chloride anions, has been prepared by contacting an LDH with molten methylphosphonic acid, and its structure solved using microcrystal X-ray diffraction at a synchrotron source.
G. B. Hix, D. S. Wragg, I. Bull, R. E. Morris and P. A. Wright, Chem. Commun., 1999, 2421 DOI: 10.1039/A907599B
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