Skip to main content
SpringerLink
Log in

X-ray diffraction structure of (5S)-3,4-dichloro-5-menthoxy-2(5H)-furanone

  • Published:
Journal of Chemical Crystallography Aims and scope Submit manuscript

Abstract

The structure of (5S)-3,4-dichloro-5-menthoxy-2(5H)-furanone is reported. The title compound crystallizes in the monoclinic space group P21: a = 6.650(2) Å, b = 8.038(3) Å, c = 14.858(8) Å, β = 97.01(3)○, V = 788.3(6) Å3, Z = 2, R = 0.0718, R w = 0.0795 for 735 observed reflections with I > 3σ (I), and the absolute configuration at C-5 of the furanone ring is shown to be (S).

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Fenske, D.; Merzweiler, K. Z. Naturforsch. 1989, 44b, 879.

    Google Scholar 

  2. Fenske, D.; Merzweiler, K. Z. Naturforsch. 1989, 44b, 884.

    Google Scholar 

  3. Yang, K.; Bott, S.G.; Richmond, M.G. Organometallics 1995, 14, 4977.

    Google Scholar 

  4. All stereochemical assignments were determined by using the Cahn–Ingold–Prelog system. See Eliel, E.L.; Wilen, S.H.; Mander, L.N. Stereochemistry of Organic Compounds, Wiley: New York, 1994; and references therein.

    Google Scholar 

  5. Shen, H.; Bott, S.G.; Richmond, M.G. J. Chem. Crystallogr. 1997, 27, 19.

    Google Scholar 

  6. Shen, H.; Bott, S.G.; Richmond, M.G. Inorg. Chim. Acta 1996, 241, 71.

    Google Scholar 

  7. Bott, S.G.; Shen, H.; Richmond, M.G. Struct. Chem. 2001, 12, 237.

    Google Scholar 

  8. Weast, R.C., Ed. 56th ed., Handbook of Chemistry and Physics, CRC Press: Cleveland, OH, 1975.

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Chemistry, University of Houston, Houston, Texas, 77204

    Simon G. Bott

  2. Department of Chemistry, University of North Texas, Denton, Texas

    Kaiyuan Yang & Michael G. Richmond

Authors
  1. Simon G. Bott
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Kaiyuan Yang
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Michael G. Richmond
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Bott, S.G., Yang, K. & Richmond, M.G. X-ray diffraction structure of (5S)-3,4-dichloro-5-menthoxy-2(5H)-furanone. Journal of Chemical Crystallography 33, 585–588 (2003). https://doi.org/10.1023/A:1024203205953

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1023/A:1024203205953

Search

Navigation