Electrochemical reduction of pyrethroid insecticides in non-aqueous solvents
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2009, Journal of Inorganic BiochemistryVoltammetric behaviour of the synthetic pyrethroid lambda-cyhalothrin and its determination in soil and well water
2004, Analytica Chimica ActaCitation Excerpt :These results demonstrate that no adsorption of lambda-cyhalothrin in the tests solutions occurred and the mass transport of electroactive species to the mercury electrode is diffusion-controlled at the three pH values tested. A study of the molecular structure of lambda-cyhalothrin together with the previous knowledge of the voltammetric behaviour of cypermethrin and deltamethrin, two pyrethroids with similar structures [12], led us to attribute the electroactivity of these insecticides in pH range 2.0–10.5 to the two-electron reduction of the double bond in the pyrethroid [16,17]. In alkaline medium (pH>10.5), the hydrolysis of the ester group in lambda-cyhalothrin [11,12] gives rise to chrysanthemum acid and 3-phenoxybenzaldehyde.
Electrochemical reduction of pyrethroid insecticides based on esters of α-cyano-3-phenoxybenzyl alcohol at glassy carbon and mercury electrodes in acetonitrile
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