Skip to main content
Log in

Cold pressed versus solvent extracted lemon (Citrus limon L.) seed oils: yield and properties

  • Original Article
  • Published:
Journal of Food Science and Technology Aims and scope Submit manuscript

Abstract

During the processing of lemon fruit, a large quantity of seeds is produced as a by-product. These seeds contain valuable components; therefore, required to be evaluated. This study aimed to compare the cold pressed with hexane-extracted lemon seed oils and determine their physicochemical and thermal properties. Cold pressing yielded significantly lower oil (36.84%) than hexane extraction (71.29%). In addition, the concentrations of free fatty acids, peroxides, and p-anisidine were lower in the cold pressed oil. Cold pressed oil showed higher total phenolics, α-tocopherol and antioxidant capacity. The major fatty acids found in the cold pressed oil were linoleic and palmitic acids, whereas β-sitosterol and campesterol were the dominant sterols. The crystallization and melting temperatures and enthalpies were also elucidated. In conclusion, this study proved that high quality of lemon seed oils can be produced by the cold pressing technique; this oil can be used in industries such as the food, cosmetic or chemical industries.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  • Abdel-Rahman AY (1980) A study on some Egyptian citrus seed oils. Grasas Aceites 31:331–333

    Google Scholar 

  • Ajewole K, Adeyeye A (1993) Characterisation of Nigerian citrus seed oils. Food Chem 47:77–78

    Article  CAS  Google Scholar 

  • Anderson D (1996) A primer on oils processing technology. In: Hui YH (ed) Bailey’s industrial oil and fat products. Wiley, New York, pp 1–60

    Google Scholar 

  • Anonymous (2016) Lemon. https://en.wikipedia.org/wiki/Lemon. Accessed 04 Jan 2016

  • Anwar F, Naseer R, Bhanger MI, Ashraf S, Talpur FN, Aladedunye FA (2008) Physico-chemical characteristics of citrus seeds and seed oils from Pakistan. J Am Oil Chem Soc 85:321–330

    Article  CAS  Google Scholar 

  • AOAC (Association of Official Analytical Chemist) (2006) Official methods of analysis of the AOAC, 18th edn. Association of Official Analytical Chemists, Washington

    Google Scholar 

  • AOCS (American Oil Chemists’ Society) (1997) Official methods and recommended practices, vol I and II, 4th edn. American Oil Chemists’ Society, Champaign

    Google Scholar 

  • Aydeniz B, Yılmaz E (2012) Enrichment of frying oils with plant phenolic extracts to extend the usage life. Eur J Lipid Sci Technol 114:933–941

    Article  CAS  Google Scholar 

  • Aydeniz B, Güneşer O, Yılmaz E (2014) Physico-chemical, sensory and aromatic properties of cold press produced safflower oil. J Am Oil Chem Soc 91:99–110

    Article  CAS  Google Scholar 

  • Bhatnagar AS, Krishna AGG (2014) Lipid classes and subclasses of cold-pressed and solvent-extracted oils from commercial Indian niger (Guizotia abyssinica (L.f.) Cass.) seed. J Am Oil Chem Soc 91:1205–1216

    Article  CAS  Google Scholar 

  • Co ED, Marangoni AG (2012) Organogels: an alternative edible oil-structuring method. J Am Oil Chem Soc 89:749–780

    Article  Google Scholar 

  • Codex (1999) Codex standard for named vegetable oils, CXSTAN 210. Turkish Food Codex, Ankara, Turkey

  • El-Adawy TA, Rahma EH, El-Bedawy AA, Gafar AM (1999) Properties of some citrus seeds. Part 3. Evaluation as a new source of protein and oil. Nahrung 43:385–391

    Article  CAS  Google Scholar 

  • Emir DD, Aydeniz B, Yılmaz E (2015) Effects of roasting and enzyme pretreatments on yield and quality of cold-pressed poppy seed oils. Turk J Agric For 39:260–271

    Article  Google Scholar 

  • Galanakis CM (2012) Recovery of high added-value components from food wastes: conventional, emerging technologies and commercialized applications. Trends Food Sci Technol 26:68–87

    Article  CAS  Google Scholar 

  • Ghazani SM, Garcia-Llatas G, Marangoni AG (2014) Micronutrient content of cold pressed, hot pressed, solvent extracted and RBD canola oil: implications for nutrition and quality. Eur J Lipid Sci Technol 116:380–387

    Article  CAS  Google Scholar 

  • Grajzer M, Prescha A, Korzonek K, Wojakowska A, Mariusz Dziadas M, Kulma A, Grajeta H (2015) Characteristics of rose hip (Rosa canina L.) cold-pressed oil and its oxidative stability studied by the differential scanning calorimetry method. Food Chem 188:459–466

    Article  CAS  Google Scholar 

  • Grilo Câmara E, Costa PN, Gurgel CSS, Beserra AFM, Almeida FNS, Dimenstein R (2014) Alpha-tocopherol and gamma-tocopherol concentration in vegetable oils. Food Sci Technol (Campinas) 34:379–385

    Article  Google Scholar 

  • Habib MA, Hammam MA, Sakr AA, Ashoush YA (1986) Chemical evaluation of Egyptian citrus seeds as potential sources of vegetable oils. J Am Oil Chem Soc 63:1192–1196

    Article  CAS  Google Scholar 

  • Hosamani KM, Sattigeri RM (2000) Industrial utilization of Rivea ornata seed oil: a moderate source of vernolic acid. Ind Crops Prod 12:93–96

    Article  CAS  Google Scholar 

  • ISO (International Standards Office) (1999) 12228:1999, Animal and vegetable fats and oils-determination of individual and total sterols contents—gas chromatographic method. International Standards Official Methods, Geneve, Switzerland

  • ISO (International Standards Office) (2000) Animal and vegetable fats and oils—Determination of unsaponifiable matter—method using diethyl ether extraction. International Standards Official Methods, Geneve, Switzerland

  • Ixtaina VY, Martinez ML, Spotorno V, Mateo CM, Maestri DM, Diehl BWK, Nolasco SM, Tomas MC (2011) Characterization of chia seed oils obtained by pressing and solvent extraction. J Food Compos Anal 24:166–174

    Article  CAS  Google Scholar 

  • Lazos ES, Servos DC (1988) Nutritional and chemical characteristics of orange seed oil. Grasas Aceites 39:232–234

    CAS  Google Scholar 

  • Malacrida CR, Kimura M, Jorge N (2012) Phytochemicals and antioxidant activity of citrus seed oils. Food Sci Technol Res 18:399–404

    Article  CAS  Google Scholar 

  • Matthaus B, Özcan MM (2012) Chemical evaluation of citrus seeds, an agro-industrial waste, as a new potential source of vegetable oils. Grasas Aceites 63:313–320

    Article  CAS  Google Scholar 

  • Minitab (2010) Minitab statistical software (version 16.1.1). Minitab Inc., State College

    Google Scholar 

  • Reda SY, Sauer EL, Batista AEC, Barana AC, Schnitzel E, Carneiro PIB (2005) Characterization of rangpur lime (Citrus limonia Osbeck) and “Sicilian” lemon (Citrus limon) seed oils, an agro-industrial waste. Cienc Tecnol Aliment 25:672–676

    Article  CAS  Google Scholar 

  • Saidani M, DhifiI W, Marzouk B (2004) Lipid evaluation of some Tunisian citrus seed. J Food Lipids 11:242–250

    Article  CAS  Google Scholar 

  • Saloua F, Eddine NI, Hedi Z (2009) Chemical composition and profile characteristics of Osage orange Maclura pomifera (Rafin.) Schneider seed and seed oil. Ind Crops Prod 29:1–8

    Article  CAS  Google Scholar 

  • SPSS (1994) SPSS professional statistics (version 10.1). SPSS Inc., Chicago

    Google Scholar 

  • Trandjiiska R, Nguyen H (1989) Triglyceride composition of seed oils from Vietnamese citrus fruits. Riv Ital Sostanze Gr 66:99–102

    Google Scholar 

  • Tuberoso CIG, Kowalczyk A, Sarritzu E, Cabras P (2007) Determination of antioxidant compounds and antioxidant activity in commercial oilseeds for food use. Food Chem 103:1494–1501

    Article  CAS  Google Scholar 

  • Yılmaz E, Arsunar ES, Aydeniz B, Güneşer O (2015a) Cold pressed capia pepperseed (Capsicum annuum L.) oils: composition, aroma and sensory properties. Eur J Lipid Sci Technol 117:1016–1026

    Article  Google Scholar 

  • Yılmaz E, Öğütcü M, Arifoglu N (2015b) Assessment of thermal and textural characteristics and consumer preferences of lemon and strawberry flavored fish oil organogels. J Oleo Sci 64:1049–1056

    Article  Google Scholar 

Download references

Acknowledgements

This study was funded by the TUBITAK (The Scientific and Technological Research Council of Turkey) and COST (European Cooperation in Science and Technology) Action TD 1203 (Food Waste Valorisation for Sustainable Chemicals, Materials and Fuels) Project No: 114O876. The authors wish to thank for financial support. We would also thank Limkon Food Industry and Trade Inc. (Adana, Turkey) for supplying the lemon seeds used in the study.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Emin Yilmaz.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Yilmaz, E., Güneşer, B.A. Cold pressed versus solvent extracted lemon (Citrus limon L.) seed oils: yield and properties. J Food Sci Technol 54, 1891–1900 (2017). https://doi.org/10.1007/s13197-017-2622-8

Download citation

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s13197-017-2622-8

Keywords

Navigation