Causes of reversible changes in the coercivity of alloys for permanent magnets as a result of cyclic heat treatment are analyzed. The magnetic properties and the metallographic and magnetic domain structures of alloy Sm(Co0.65Fe0.26Cu0.07Zr0.02)7 are studied as a function of the temperature of interruption of the process cooling. The own results and data of foreign authors are used for developing a scheme of the processes occurring in the alloy in order to explain the mechanism of the “damage – restoration” phenomenon in alloys of the Sm – Co – Cu – Fe – Zr system of type Sm(Co0.65Fe0.26Cu0.07Zr0.02)7.
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A. S. Lileev, V. V. Pinkas, K. V. Voronchihina, and A. V. Gunbin, “Research of reversibility of coercivity under heat treatment in permanent magnets,” in: Moscow International Symposium on Magnetism (MISM), 1 – 5 July, 2017, Moscow, Book of Abstracts, p. 826.
A. S. Lileev, V. P. Menushenkov, and V. I. Sumin, “Investigation of reversible changes of magnetic properties in alloy YuNDK35T5 after a “damage – restoration” heat treatment,” Fiz. Met. Metalloved., 36(1), 183 – 186 (1973).
B. G. Livshits, A. S. Lileev, and V. P. Menushenkov, “Reversibility of magnetic properties of sintered permanent magnets from SmCo5 compound,” Metally, No. 4, 161 – 164 (1976).
T. G.Woodcock, F. Bittner, T. Mix, et al., “On the reversible and fully repeatable increase in coercive field of sintered Nd – Fe – B magnets following post sinter annealing,” J. Magn. Magn. Mater., 360, 154 – 157 (2014).
X. Y. Xiong, T. Ohkubo, T. Koyama, et al., “The microstructure of sintered Sm(Co0.72Fe0.20Cu0.055Zr0.025)7.5 permanent magnet studied by atom probe,” Acta Mater., 52, 737 – 748 (2004).
O. A. Arinicheva, A. S. Lileev, M. Raizner, et al., “Effect of cyclic heat treatment in the range of 800 – 400°C on the properties of sintered magnets based on alloy Sm(Co, Fe, Cu, Zr)z,” Metalloved. Term. Obrab. Met., No. 11, 16 – 20 (2014).
O. Gutfleisch, K.-H Muller, K. Khlopkov, et al., “Evolution of magnetic domain structures and coercivity in high-performance SmCo 2:17-type permanent magnets,” Acta Mater., 54, 997 – 1008 (2006).
R. Gopalan, K. Hono, A. Yan, and O. Gutfleisch, “Direct evidence for Cu concentration and its correlation to coercivity in Sm(Co0.74Fe0.1Cu0.12Zr0.4)7.4 ribbons,” Scr. Mater., 60, 764 – 767 (2009).
H. Sepehri-Amin, J. Thielsch, J. Fischbacher et at., “Correlation of microchemistry of cell boundary phase and interface structure to the coercivity of Sm(Co0.784Fe0.100Cu0.088Zr0.028)7.19 sintered magnets,” Acta Mater., 126, 1 – 10 (2017).
C. Tikadzumi, The Physics of Ferromagnetism. Magnetic Characteristics and Applications [Russian translation], Mir, Moscow (1987), 420 p.
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Translated from Metallovedenie i Termicheskaya Obrabotka Metallov, No. 8, pp. 4 – 8, August, 2018.
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Lileev, A.S., Pinkas, V.V., Voronchikhina, K.V. et al. Reversible Changes of Coercive Force in Sm – Co – Cu – Fe – Zr Alloy for Permanent Magnets Under Cyclic Heat Treatment. Met Sci Heat Treat 60, 489–493 (2018). https://doi.org/10.1007/s11041-018-0306-2
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DOI: https://doi.org/10.1007/s11041-018-0306-2