Skip to main content

Advertisement

Log in

Rapid synthesis of tunable-structured short-pore SBA-15 and its application on CO2 capture

  • Published:
Journal of Porous Materials Aims and scope Submit manuscript

Abstract

The well-ordered hexagonal short-pore SBA-15 (SSBA-15) has been successfully synthesized via an energy-efficient process under the microwave-hydrothermal condition, in which the formation duration [stirring duration (ripening step) and microwave-hydrothermal treatment duration (aging step)] has been greatly decreased from 48 h for conventional hydrothermal treatment to <2 h. The extension of the ripening duration led to the evidently improved uniformity and regularity of particles while the increase of aging duration resulted in less intrawall pores and more structural mesopores. The optimal condition to get highly ordered SSBA-15 in this work was the duration of 2 h for both steps, and the SSBA-15 obtained was composed of cuboid-like particles, whose pore length was ca. 450 ± 50 nm and pore size was around 10 nm. The SSBA-15 was modified with different amine agents to prepare solid amine adsorbent, the obtained adsorbents showed considerable CO2 adsorption ability, indicating that this fast-prepared SSBA-15 can be a promising support of CO2 adsorbents.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Scheme 1
Fig. 4
Fig. 5
Fig. 6
Scheme 2
Fig. 7
Fig. 8

Similar content being viewed by others

References

  1. J.M. Rosenholm, M. Linde´n, J. Control. Release. 128, 157 (2008)

    Article  CAS  Google Scholar 

  2. J.T. Dama, D. Badloea, A. Ramanathanb, K. Djanashvilia, F. Kapteijnc, U. Hanefelda, Appl. Catal. A Gen. 468, 150 (2013)

    Article  CAS  Google Scholar 

  3. S. Telalovic, A.N.J. Ramanathan, R. Maheswari, C. Kwakernaak, F. Soulimani, H.C. Brouwer, G.K. Chuah, B.M. Weckhuysen, U. Hanefeld, Chem. Eur. J. 17, 2077 (2011)

    Article  CAS  Google Scholar 

  4. A. Ramanathan, M.C.C. Villalobos, C. Kwakernaak, S. Telalovic, U. Hanefeld, Chem. Eur. J. 14, 961 (2008)

    Article  CAS  Google Scholar 

  5. S.S.P. Eloy, O.M. Mara, A. Amaya, S. Raul, C. Guillermo, M.V. Mercedes, Int. J. Greenh. Gas. Control 17, 366 (2013)

    Article  CAS  Google Scholar 

  6. H.G. Aliakbar, Y. Yong, S. Abdelhamid, Energy Fuel. 25, 4206 (2011)

    Article  CAS  Google Scholar 

  7. H. Norihito, Y. Katsunori, Y. Tatsuaki, Micropor. Mesopor. Mater. 84, 357 (2005)

    Article  CAS  Google Scholar 

  8. Z. Kake, Y. Bin, Z. Wuzong, H. Heyong, Chem. Commun. (1), 98 (2003)

  9. A. Martı´n, R.A. Garcı´a, D. Sen Karaman, J.M. Rosenholm, J. Mater. Sci. 49, 1437 (2014)

    Article  CAS  Google Scholar 

  10. Z. Qing-Zhou, W. Yan-Ying, W. Xiao-Han, J. Incl. Phenom. Macrocycl. Chem. 77, 113 (2013)

    Article  CAS  Google Scholar 

  11. K. Parveen, V. Vadim, Micropor. Mesopor. Mater. 132, 1 (2010)

    Article  CAS  Google Scholar 

  12. Z. Runduo, S. Dongjun, L. Ning, C. Yu, C. Biaohua, Appl. Catal. B Environ. 146, 79 (2014)

    Article  CAS  Google Scholar 

  13. C. Yu, B. Tian, J. Fan, G.D. Stucky, D. Zhao, Chem. Commun. (24), 2726 (2001)

  14. D.Y. Zhao, Q.S. Huo, J.L. Feng, J. Am. Chem. Soc. 120, 6024 (1998)

    Article  CAS  Google Scholar 

  15. R. Ryoo, C.H. Ko, M. Kruk, J. Phys. Chem. B 104, 11465 (2000)

    Article  CAS  Google Scholar 

  16. L. Cao, M. Kruk, J. Colloid Interface Sci. 361, 472 (2011)

    Article  CAS  Google Scholar 

  17. Z. He, S. Junming, M. Ding, W. Gisela, S.S. Dang, B. Xinhe, J. Phys. Chem. B 110, 25908 (2006)

    Article  CAS  Google Scholar 

  18. S.W. Patrick, W.L. Wayne, D.Y. Zhao, Y. Peidong, F. Bradley, G.D. Chmelka, J. Am. Chem. Soc. 121, 254 (1999)

    Article  Google Scholar 

  19. Z. He, S. Junming, M. Ding, B. Xinhe, K.H. Achim, W. Giesela, S. Dangsheng, S. Robert, J. Am. Chem. Soc. 126, 7440 (2004)

    Article  CAS  Google Scholar 

  20. K. Sridhar, V.C. Menon, Mater. Lett. 27, 313 (1996)

    Article  Google Scholar 

  21. L. Bharat, S.K. Newalkar, K. Hiroaki, Chem. Commun. (23), 2389 (2000)

  22. P. Cyril, W. Karen, F.L. Adam, Green Chem. 16, 197 (2014)

    Article  Google Scholar 

  23. C.S. Cundy, C. Collect, Chem. Commun. 63, 1699 (1998)

    CAS  Google Scholar 

  24. L. Bharat, K. Newalkar, K. Sridhar, Chem. Commun. (16), 1774 (2002)

  25. K.H. Young, C. Jong-San, K. Young-Uk, P. Sang-Eon, Micropor. Mesopor. Mater. 68, 21 (2004)

    Article  CAS  Google Scholar 

  26. L. Bharat, J.O. Newalkar, K. Sridhar, J. Phys. Chem. B 105, 8356 (2001)

    Article  CAS  Google Scholar 

  27. M. Kruk, L. Cao, Langmuir 23, 7247 (2007)

    Article  CAS  Google Scholar 

  28. G.K. Young, S.S. Seung, S.C. Ung, J. Colloid Interface Sci. 361, 594 (2011)

    Article  CAS  Google Scholar 

  29. B. Taissire, V. Loïc, L. Bénédicte, M. Claire, Micropor. Mesopor. Mater. 153, 100 (2012)

    Article  CAS  Google Scholar 

  30. J.M. Sun, H. Zhang, D. Ma, Y. Chen, X.H. Bao, A. Klein-Hoffmann, N. Pfänder, D.S. Su, Chem. Commun. (42), 5343 (2005)

  31. V.L. Zholobenko, A.Y. Khodakov, D. Durand, Micropor. Mesopor. Mater. 66, 297 (2003)

    Article  CAS  Google Scholar 

  32. K.S.W. Sing, D.H. Everett, R.A.W. Haul, L. Moscou, R.A. Pierotti, J. Rouquerol, T. Siemieniewska, Pure Appl. Chem. 57, 603 (1984)

    Google Scholar 

  33. K. Tomas, R. Nina, S. Motolani, S. Jan-Henrik, L. Mika, A. Viveka, Chem. Mater. 25, 1989 (2013)

    Article  CAS  Google Scholar 

  34. A. Galarneau, H. Cambon, F.D. Renzo, R. Ryoo, M. Choi, F. Fajula, New J. Chem. 27, 73 (2003)

    Article  CAS  Google Scholar 

  35. L. Peter, R.R. Adrian, Z. Malin, A. Viveka, Langmuir 25, 4685 (2009)

    Article  CAS  Google Scholar 

  36. H.G. Aliakbar, Y. Yong, S. Abdelhamid, Energy Fuels 25, 4206 (2011)

    Article  CAS  Google Scholar 

  37. B. Santiago, F.V. Lourdes, Langmuir 29, 199 (2013)

    Article  CAS  Google Scholar 

Download references

Acknowledgments

The authors gratefully acknowledge the financial support provided by the National Natural Science Foundation of China (Grant No. 51473187).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Shuixia Chen.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Ma, B., Zhuang, L. & Chen, S. Rapid synthesis of tunable-structured short-pore SBA-15 and its application on CO2 capture. J Porous Mater 23, 529–537 (2016). https://doi.org/10.1007/s10934-015-0106-7

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10934-015-0106-7

Keywords

Navigation