Abstract
Nanoscale SrHPO4 is prepared via a polyol-mediated synthesis. The resulting particles are well crystallized, non-agglomerated, and very uniform in size and shape. By adjusting the experimental conditions, SrHPO4 can be obtained with the α-type as well as with the β-type of modification. In particular, particle diameters of 16 nm (α-SrHPO4) and 12 nm (β-SrHPO4) are obtained. The title compound is characterized by scanning electron microscopy, dynamic light scattering, X-ray powder diffraction, and infrared spectroscopy.
Similar content being viewed by others
References
Fischer A, Mallat T, Baiker A (1997) Catal Today 37:167. doi:https://doi.org/10.1016/S0920-5861(97)00009-6
Louati B, Guidara K, Gargouri M, Fourati M (2005) Z Naturforsch 60a:121
Kim J, Noh M, Cho J, Kim HM, Kim KB (2005) J Electrochem Soc 152:A1142. doi:https://doi.org/10.1149/1.1896526zz
Levchik SV, Weil ED (2006) J Fire Sci 24(5):364. doi:https://doi.org/10.1177/0734904106068426
Boudjada A, Masse R, Guitel JC (1978) Acta Crystallogr B 34:2692. doi:https://doi.org/10.1107/S0567740878009036
Taher LB, Smiri L, Laligant Y, Maisonneuve V (2000) J Solid State Chem 152:428. doi:https://doi.org/10.1006/jssc.2000.8700
Purnendu P, Ray AR, Ramanan A (2007) J Am Ceram Soc 90(4):1237. doi:https://doi.org/10.1111/j.1551-2916.2007.01508.x
Purnendu P, Ramanan A, Ray AR (2006) Am J Biochem. Biotechnol 2(2):61
Zheng Y, Cheng Y, Wang Y, Yu Y, Chen D, Bao F (2005) J Cryst Growth 280:569. doi:https://doi.org/10.1016/j.jcrysgro.2005.03.067
Toneguzzo P, Viau G, Acher O, Guillet F, Bruneton E, Fievet F (2000) J Mater Sci 35:3767. doi:https://doi.org/10.1023/A:1004864927169
Feldmann C, Jungk HO (2001) Angew Chem Int Ed 40:359. doi:10.1002/1521-3773(20010119)40:2<359::AID-ANIE359>3.0.CO;2-B
Feldmann C, Roming M, Trampert K (2006) Small 2:1248. doi:https://doi.org/10.1002/smll.200600140
LaMer VK, Dinegar RH (1950) J Am Chem Soc 72:4847. doi:https://doi.org/10.1021/ja01167a001
Aia MA, Mathers JE, Mooney RW (1964) J Chem Eng Data 9:335. doi:https://doi.org/10.1021/je60022a006
Mooney RW, Aia MA, Hoffman CWW, Ropp RC (1959) J Am Chem Soc 81:827. doi:https://doi.org/10.1021/ja01513a020
Ostwald W (1897) Z Phys Chem 22:289
Ropp RC, Aia MA, Hoffman CWW, Veleker TJ, Mooney RW (1959) Anal Chem 31:1163. doi:https://doi.org/10.1021/ac60151a026
Boudjada A, Masse R, Guitel JC (1978) Acta Crystallogr B 34:2692. doi:https://doi.org/10.1107/S0567740878009036
Mel’nikova RY, Dzyuba ED, Pechkovskii VV, Barannikova TI, Kovalishina VI (1982) Russ J Inorg Chem 27:1724
Weidlein J, Müller U, Dehnicke K (1988) Schwingungsspektroskopie. Thieme Verlag, Stuttgart
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Roming, M., Feldmann, C. Selective synthesis of α- and β-SrHPO4 nanoparticles. J Mater Sci 43, 5504–5507 (2008). https://doi.org/10.1007/s10853-008-2830-8
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10853-008-2830-8