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Special Features of X-ray Analysis of Cellulose Crystallinity and Content in Flax Fibres

  • MATERIALS SCIENCE
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Fibre Chemistry Aims and scope

Experimental X-ray diffraction analysis procedures and calculation algorithms are proposed for determining the degree of crystallinity of flax fibres of varied purity and their cellulose component from the integral values of diffraction by the crystallite regions of the analysis sample and the reference standard, which are normalized, taking account of the scattering mass of the preparations. The possibility of determination of the mass cellulose content in flax fibres by X-ray analysis, which dispenses with the need for labor and time consuming chemical analyses, is substantiated.

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This work was carried out with the financial support of the Russian Foundation for Fundamental Research (Project No. 15-48-03021r_tsentr-_a) using equipment of the Center for Collective Utilization of IGKhTU (Ivanovo State University of Chemistry and Technology).

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Authors and Affiliations

  1. G. A. Krestov Institute of Chemistry of Solutions, Russian Academy of Sciences, Ivanovo, Russia

    A. P. Moryganov & V. G. Stokozenko

  2. Ivanovo State University of Chemistry and Technology, Ivanovo, Russia

    A. E. Zavadskii

Authors
  1. A. P. Moryganov
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  2. A. E. Zavadskii
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  3. V. G. Stokozenko
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Correspondence to A. P. Moryganov.

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Translated from Khimicheskie Volokna, No. 6, pp. 33-38, November-December, 2017

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Moryganov, A.P., Zavadskii, A.E. & Stokozenko, V.G. Special Features of X-ray Analysis of Cellulose Crystallinity and Content in Flax Fibres. Fibre Chem 49, 382–387 (2018). https://doi.org/10.1007/s10692-018-9904-4

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  • DOI: https://doi.org/10.1007/s10692-018-9904-4

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