Abstract
This paper studies the influence of ripening stage and maceration time (1–23 days) on the contribution of each cluster grape components to phenolic composition and astringency in wine-simulated macerations. In general terms, proanthocyanidin extraction from skins, stems and especially from seeds increased with maceration time. The ripening stage also had a major influence on tannin extraction and astringency. The tannin contribution from skins and stems increased with ripening but the contribution from the seeds decreased. The contribution to astringency from all cluster components was clearly higher when the grapes were unripened. The mean degree of polymerization of the tannins from skin and seed components was unaffected by ripening and maceration length.
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References
Arnold R, Noble AC (1978) Bitterness and astringency of grape seed phenolics in a model solution. Am J Enol Vitic 29:150–152
Noble AC (1990) Bitterness and astringency in wine: development in food science 25. In: Rouseff RL (eds) Bitterness in foods and beverages. Elsevier, New York, pp 145–158
Gawel R (1998) Red wine astringency: a review. Austr J Grape Wine Res 4:74–98
Vidal S, Francis L, Guyot S, Marnet N, Kwiatkowski M, Gawel R, Cheynier V, Waters EJ. (2003) The mouth-feel properties of grape and apple proanthocyanidins in a wine-like medium. J Sci Food Agric 83(6):564–573
Lea A, Bridle P, Timberlake C, Singlentong VL (1979) The procyanidins of white grape and wines. Am J Enol Vitic 38:277–281
Czochanska Z, Foo L, Porter L (1979) Compositional changes in lower molecular weight flavan during grape maturation. Phytochemistry 18:1819–1822
Glories Y (1984) La couleur des vins rouges. 1ère partie: Les equilibres des anthocyanes et des tannins. Connaiss Vigne Vin 18:195–217
Bourzeix M, Weyland D, Héredia N, Desfeux C (1986) Étude des catéchines et des procyanidols de la grape de raisin du vin et d’autres dérivés de la vigne. Bulletin O.I.V.:669–670, 1179–1254
Ribéreau-Gayon P, Glories Y, Maujean A, Dubourdieu D (2000) The chemistry of wine stabilisation and treatments. In: Handbook of enology, vol 2. Wiley, Chichester, pp 232–234
Prieur C, Rigaud J, Cheynier V, Moutounet M (1994) Oligomeric and polymeric procyanidins from grape seeds. Phytochemistry 36:781–784
Kennedy JA, Matthewa MA, Waterhouse AL (2002) Effect of maturity and vine water status on grape skin and wine flavonoides. Am J Enol Vitic 53(4):268–274
Souquet J-M, Cheynier V, Brossaud F (1996) Moutounet, M. Polimeric Proanthocyanidins from grape skins. Phytochemistry 43:509–512
Gonzalez-Manzano S, Rivas-Gonzalo JC, Santos-Buelga C (2004) Extraction of flavan-3-ols from grape seed and skin into wine using simulated maceration. Anal Chim Acta 513:283–289
Souquet JM, Cheynier V, Moutonet M (2000) Les proanthocyanidins du raisin. Bulletin de l’OIV 73:601–609
Vivas N, Nonier MF, Vivas de Gaulejac N, Absalon C, Bertrand A, Mirabel M (2004) Differentiation of proanthocyanidin tannins from seeds, skins and stems of grape (Vitis vinifera) and heatwood of Quebracho (Shinopsis balansae) by matrix assisted laser desorption/ ionisation time of flight mass spectrometry and thioacidolysis/liquid chromatography/electrospray ionisation mass spectrometry. Anal Chim Acta 513:147–156
Moutonet M, Fulcrand H, Sarni-Manchado P, Souquet JM, Atanalsova V, Labarbe B, Maury C, Vidal S, Cheynier V (2002) Wine tanins and their role in astringency perception. In: 13ème Symposium International d’œnologie, Montpellier, pp 737–747
Sun B, Spranger MI (2005) Changes in phenolic composition of Tinta Miúda red wines after 2 years of ageing in bottle: effect of winemaking Technologies. Eur Food Res Technol 221:305–312
Vivas N, Glories Y (1996) Role of oak wood ellagitannins in the oxidation process of red wines during aging. Am J Enol Vitic 47:103–107
Vidal S, Francis L, Noble A, Kwiatkowski M, Cheynier V, Waters E (2004) Taste and mouth-feel properties of different types of tannin-like polyphenolic compounds and anthocyanins in wine. Anal Chim Acta 513:57–65
Herderich MJ, Smith PA (2005) Analysis of grape and wine tannins: methods, applications and challenges. Austr J Grape Wine Res 11:205–214
Ryan JM, Revilla E (2003) Anthocyanin composition of Cabernet sauvignon and Tempranillo grapes at different stages of ripening. J Agric Food Chem 51:3372–3378
Ó-Marques J, Reguinga R, Laureano O, Ricardo-da-Silva JM (2005) Changes in grape seed, skins and pulp condensed tannins during berry ripening: effect of fruit pruning. Ciência Tècnica Vitivinicola 20(1):35–52
Peyrot des Gachons C, Kennedy JA (2003) Direct method determining seed and skin proanthocyanidin extraction into red wine. J Agric Food Chem 51:5877–5881
Canals R, Llaudy MC, Valls J, Canals JM, Zamora F (2005) Influence of ethanol concentration on the extraction of color and phenolic compounds from the skin and seed of Tempranillo grapes at different stages of ripening. J Agric Food Chem 53:4019–4025
Romeyer FM, Macheix JJ, Sapis JC (1986) Changes and importance of oligomeric procyanidins during maturation of grape seed. Phytochemistry 25(1):219–221
Boulton RB, Singleton VL, Bisson LF, Kunkee RE (1995) Principles practices of winemaking. Chapman and Hall, New York, p 88
Hashizume K, Samuta T (1997) Green odorant of grape cluster stem and their ability to cause wine stemmy flavor. J Agric Food Chem 45:1333–1337
Blouin (2000) La vinificación bordelesa de las uvas tintas. In: Madrid AMV (ed) Enología: Fundamentos Científicos Tecnológicos. Cord, Flanzys, pp 465–467
Delteil D (2000) El despalillado de las uvas. In: Madrid AMV (eds) Enología: Fundamentos Científicos Tecnológicos. Cord, Flanzys, pp 436–437
Peynaud E (1984) Connaissance et travail du vin. Dunod, Bordas, Paris, pp 133–135
Peynaud E (1988) Le vin et les jours. Dunod, Bordas, Paris, pp 228–232
Ricardo da Silva JM, Rigaud J, Cheynier V, Cheminat A, Moutountet M (1991)Procyanidin dimers and trimers from grape seeds. Phytochemistry 30(4):1259–1264
Jordao A, Ricardo da Silva J, Laureano O (2001) Evolution of catechins and oligomeric proacyanidins during grape maturation of Castelao Frances and Touriga Francesa. Am J Enol and Vitic 52(3):230–234
Jackson DI, Lombard PB (1993) Environmental and management practices affecting grape composition and wine quality. A review. Am J Enol Vitic 44:409–430
Esteban MA, Villanueva MJ, Lissarrague JR (2001) Effect of irrigation on changes in the anthocyanins composition of the skin of cv Tempranillo (Vitis vinifera L) grape berries during ripening. J Sci Food Agric 81:409–420
Vivas de Gaulejac N, Nonier MF, Guerra C, Vivas N (2001) Anthocyanins in grape skins during maturation of Vitis vinifera L cv Cabernet sauvignon and Merlot noir from different Bourdeaux terroirs. Journal International de la Vigne et du Vin 35(3):149–156
Pérez-Magariño S, González San-José ML (2004) Evolution of flavanoles, anthocyanins and their derivatives during the aging red wine elaborated from grape harvested at differents stage of ripening. J Agric Food Chem 52:1181–1189
Gómez- Plaza E, Gil- Muñoz R., López- Roca JM, Martínez- Cutillas A, Fernández- Fernández JI (2001) Phenolic compounds and colour stability of red wines: effect of skin maceration time. Am J Enol Vitic 53(3):266–270
Zimman A, Joslin WS, Lyon ML, Meier J, Waterhouse AL(2002) Maceration variables affecting Phenolic composition in commercial-scale Cabernet sauvignon winemaking trials. Am J Enol Vitic 53(2):93–98
Gómez- Míguez M, Heredia FJ (2004) Effect of the maceration technique on the relationships between anthocyanins composition and objective color of Syrah wines. J Agric Food Chem 52:5117–5123
Kelebek H, Canbas A, Selli S, Saucier C, Jourdes M, Glories Y (2005) Influence of different maceration times on the anthocyanin composition of wine mades from Vitis vinifera cvs Bogazkere and Öküzgözü. J Food Eng. doi:10.1016/j.jfoodeng.2005.08.032
Kennedy JA, Mattehus MA, Waterhouse AL (2000) Changes in grape seed polyphenols during fruit ripening. Phytochemistry 55:77–85
Kennedy JA, Troup GL, Pilbrow JR, Hutton DR, Hewitt D, Hunter CR, Ristic R, Iland PG, Jones GP (2000) Development of seed polyphenols in berries from Vitis vinifera L. cv. Shiraz. Austr J Grape Wine Res 6:244–254
Jordao A, Ricardo da Silva J, Laureano O (2001) Evolution of proanthocyanidins in bunch stems during berry development (Vitis vinifera L.). Vitis 40:17–22
Harbertson JF, Kennedy JA, Adams DO (2002) Tannin in skins and seeds of cabernet sauvignon, Syrah and Pinot noir berries during ripening. Am J Enol Vitic 53(1):54–59
O.I.V. (2005) Le recueil des méthodes internationales d’analyse des vins et des moûts, vols I, II, Sect 3. O.I.V, Paris
Niketic-Aleksic GK, Hrazdrina G (1972) Quantitaive analysis of the anthocyanin content in grape juices and wine. Lebensmittel-Wissenschaft & Technologie 5(5):163–165
Ribéreau-Gayon P, Stonestreet E (1966) Dosage des tanins du vin rouge et determination de leur structure. Chim Anal 48:188–196
Nagel CW, Glories Y (1991) Use of a modified dimethylaminocinnamaldehyde reagent for analysis of flavanols. Am J Enol Vitic 42:364–366
Rodríguez M, Lezáun J, Canals R, Llaudy MC, Canals JM, Zamora F (2005) Influence of the presence of the lees during oak ageing on colour and phenolic compounds composition of red wine. Food Sci Technol Int 11(4):289–296
Llaudy MC, Canals R, Canals JM, Rozès N, Arola Ll, Zamora F (2004) New method for evaluating astringency in red wine. J Agric Food Chem 52:742–746
Mazza G, Fukumoto L, Delaquis P, Girard B, Ewert B (1999) Anthocyanins, phenolic and color of Cabernet franc, Merlot and Pinot noir from British Columbia. J Agric Food Chem 47:4009–4017
Spranger MI, Climaco MC, Sun B, Eiriz N (2004) Differentiation of red winemaking technologies by phenolic and volatile composition. Anal Chim Acta 513:151–161
Geny L, Saucier C, Bracco S, Daviaud F, Glories Y (2003) Composition and cellular localization of tannins in grape seeds during maturation. J Agric Food Chem 51:8051–8054
Fuster A (2001) Les polysaccharides, leur contribution à la qualité du vin. Revue Française d’Oenologie 187:14–17
Vidal S, Courcoux P, Francis L, Kwiatkowski M, Gawel R, Williams P, Waters E, Cheynier V (2004) Use of an experimental design approach for evaluation key wine components on mouth-feel perception. Food Qual Prefer 15:219–217
Mateus N, Carvalho E, Luis C, de Freitas V (2004) Influence of the tannin structures on the disruption of carbohydrates on protein–tannin aggregates. Anal Chim Acta 513:135–140
Acknowledgments
We thank Centro de Investigación Científica y Tecnológica (AGL 2001–0716 and AGL 2004-02309) and the Departament d’Universitats, Recerca i Societat de la Informació de la Generalitat de Catalunya for financial support. We also thank René Barbier (Clos Mogador) for providing the grapes for the experiments.
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del Llaudy, M.C., Canals, R., Canals, J.M. et al. Influence of ripening stage and maceration length on the contribution of grape skins, seeds and stems to phenolic composition and astringency in wine-simulated macerations. Eur Food Res Technol 226, 337–344 (2008). https://doi.org/10.1007/s00217-006-0542-3
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DOI: https://doi.org/10.1007/s00217-006-0542-3