Skip to main content
SpringerLink
Log in

A theoretical application of SEMUT NMR spectroscopy to deuterated compounds

  • Published:
Applied Magnetic Resonance Aims and scope Submit manuscript

Abstract

The product operator formalism is widely used for analytical description of multiple-pulse nuclear magnetic resonance (NMR) experiments for weakly coupled spin systems.13C subspectral editing with a multiple quantum trap (SEMUT) NMR spectroscopy is used for subspectral editing of CH3, CH2, CH and C groups. In this study, after obtaining the evolutions of IxS 2y and IyS 2y product operators under the spin-spin coupling Hamiltonian forIS (I = 1/2,S = 1) spin system, the product operator technique was applied for the analytical description of13C SEMUT NMR for CDn groups. Then, theoretical discussion and experimental suggestions for the subspectral editing of CD3, CD2, CD and C groups are presented.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Sørensen O.W., Eich G.W., Levitt M.H., Bodenhausen G., Ernst R.R.: Prog. NMR Spectrosc.16, 163–192 (1983)

    Article  Google Scholar 

  2. Van de Ven F.J.M., Hilbers C.W.: J. Magn. Reson.54, 512–520 (1983)

    Google Scholar 

  3. Packer K.J., Wright K.M.: Mol. Phys.50, 797–813 (1983)

    Article  ADS  Google Scholar 

  4. Shriver J.: Concepts Magn. Reson.4, 1–33 (1992)

    Article  Google Scholar 

  5. Howarth M.A., Lian L.Y., Hawkes G.E., Sales K.D.: J. Magn. Reson.68, 433–452 (1986)

    Google Scholar 

  6. Ernst R.R., Bodenhausen G., Wokaun A.: Principles of Nuclear Magnetic Resonance in One and Two Dimensions. Oxford: Clarendon Press 1987.

    Google Scholar 

  7. Chandrakumar N., Subramanian S.: Modern Techniques in High Resolution FT NMR. New York: Springer 1987.

    Google Scholar 

  8. Gençten A., Köksal F.: Spectrosc. Lett.30, 71–78 (1997)

    Article  ADS  Google Scholar 

  9. Gençten A., Özdoğan T., Köksal F.: Spectrosc. Lett.31, 981–987 (1998)

    Article  ADS  Google Scholar 

  10. Bildsøe H., Dønstrup S., Jakobsen H.J., Sørensen O.W.: J. Magn. Reson.53, 154–162 (1983)

    Google Scholar 

  11. Bendall M.R., Pegg T.D.: J. Magn. Reson.59, 237–249 (1984)

    Google Scholar 

  12. Sørensen U.B., Bildsøe H., Jakobsen H.J., Sørensen O.W.: J. Magn. Reson.65, 222–238 (1985)

    Google Scholar 

  13. Bendall M.R, Pegg T.D.: J. Magn. Reson.52, 164–168 (1983)

    Google Scholar 

  14. Bendall M.R., Pegg T.D., Tyburn G.M., Brevard C.: J. Magn. Reson.55, 322–328 (1983)

    Google Scholar 

  15. Chanrakumar N.: J. Magn. Reson.63, 174–178 (1985)

    Google Scholar 

  16. Nakashima T.T., McClung R.E.D., John B.K.: J. Magn. Reson.58, 27–36 (1984)

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Physics, Faculty of Arts and Sciences, Ondokuz Mayıs University, Samsun, Turkey

    A. Gençten, Ö. Tezel & A. Köroğlu

Authors
  1. A. Gençten
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Ö. Tezel
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. A. Köroğlu
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Gençten, A., Tezel, Ö. & Köroğlu, A. A theoretical application of SEMUT NMR spectroscopy to deuterated compounds. Appl. Magn. Reson. 20, 265–273 (2001). https://doi.org/10.1007/BF03162325

Download citation

  • Received:

  • Revised:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF03162325

Keywords

Search

Navigation