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Molecular and crystal structure of 1,4-diacethoxy naphthalene: Structural analysis of methyl substituted 1,4-diacethoxynaphthalenes

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Abstract

Methyl substituted 1,4-diacethoxynaphthalenes have been synthetized and analyzed by means of ultraviolet and1H-nmr. Positional effects of the methyl substitution on the spectroscopic parameters have been rationalized. 6,7-Dimethyl-1,4-diacethoxynaphthalene,V, has been analyzed by X-ray diffraction techniques. Crystals are monoclinic P21,a=8.816(1),b=26.676(7),c=6.189(1) Å,β=103.9 (2) ° and four molecules in the unit cell.

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Authors and Affiliations

  1. Departamento de Química, Cl, Facultad de Ciencias, Universidad Autónoma de Madrid, Canto Blanco, 28049, Madrid, Spain

    José Gonzalo Rodríguez & Alfonso de Pablo

  2. Departamento de Rayas X, Instituto Rocasolano, C. S. I. C., Serrano 119, 28006, Madrid, Spain

    Julian Lopez de Lerma & Aurea Perales

Authors
  1. José Gonzalo Rodríguez
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  2. Alfonso de Pablo
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  3. Julian Lopez de Lerma
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  4. Aurea Perales
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Rodríguez, J.G., de Pablo, A., de Lerma, J.L. et al. Molecular and crystal structure of 1,4-diacethoxy naphthalene: Structural analysis of methyl substituted 1,4-diacethoxynaphthalenes. Journal of Crystallographic and Spectroscopic Research 19, 307–316 (1989). https://doi.org/10.1007/BF01194126

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  • DOI: https://doi.org/10.1007/BF01194126

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