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Role of Silicon Carbide in Phase-Evolution and Oxidation Behaviors of Pulse Electrodeposited Nickel-Tungsten Coating

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Abstract

Silicon carbide (SiC) was reinforced in the pulse electrodeposited nickel-tungsten (Ni-W) coatings deposited on the steel substrate, and isothermal oxidation test was performed at 1273 K (1000 °C) for 24 hours. Addition of just 2 vol pct of SiC showed 26 pct increase in the relative oxidation resistance of Ni-W coating. The increased oxidation resistance was attributed to the phase evolution (SiO2, Cr2O3, CrSi2, Ni2SiO4, Cr7C3, Cr3C2, and Cr3Si), which suppressed the spallation of the oxide scale in Ni-W-2 vol pct SiC. The presence of Fe2O3 phase in the oxidized Ni-W coating was mainly responsible for the major multiple spallations at the interface and in the bulk, which resulted in the degradation of oxidation resistance.

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Acknowledgments

The authors at the Indian Institute of Technology, Patna (IIT-P) thank Dr. Srinivasa Rao Bakshi, Assistant Professor, the Department of Metallurgical and Materials Engineering, the Indian Institute of Technology, Madras (IIT-M) for providing XRD characterization facility. The authors also thank the DST-SERB (Grant No. SB/FTP/ETA-0350/2013) for their support and assistance in respect of this project.

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Authors and Affiliations

  1. Department of Materials Science and Engineering, Indian Institute of Technology Patna, Bihta Kanpa Road, Bihta, Patna, Bihar, 801103, India

    M. Sribalaji (PhD Research Scholar), O. S. Asiq Rahman (PhD Research Scholar) & Anup Kumar Keshri (Assistant Professor)

  2. Madanjeet School of Green Energy Technologies, Centre for Nanoscience and Technology, Pondicherry University, Puducherry, 605014, India

    P. Arun Kumar (PhD Research Scholar) & K. Suresh Babu (Assistant Professor)

  3. International Advanced Research Centre for Powder Metallurgy & New Materials (ARCI), Balapur P.O., Hyderabad, Andhra Pradesh, 500005, India

    Nitin P. Wasekar (Scientist) & G. Sundararajan (Professor)

  4. Indian Institute of Technology Madras, Chennai, India

    G. Sundararajan (Professor)

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  1. M. Sribalaji
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  2. O. S. Asiq Rahman
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Correspondence to Anup Kumar Keshri.

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Manuscript submitted July 27, 2016.

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Sribalaji, M., Asiq Rahman, O.S., Arun Kumar, P. et al. Role of Silicon Carbide in Phase-Evolution and Oxidation Behaviors of Pulse Electrodeposited Nickel-Tungsten Coating. Metall Mater Trans A 48, 501–512 (2017). https://doi.org/10.1007/s11661-016-3847-2

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