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Effect of Temperature on the Loss of Ductility of S-135 Grade Drill Pipe Steel and Characterization of Corrosion Products in CO2 Containing Environments

  • Symposium: Fatigue & Corrosion Damage in Metallic Materials
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Abstract

Evaluation of loss of ductility of the API S-135 grade drill pipe steel was studied at different temperatures from 298 K to 448 K (25 °C to 175 °C) in CO2 containing solution using a constant extension rate test in connection with a high-temperature/high-pressure autoclave. The effect of temperature on the composition and morphology of corrosion product layers of this steel were also investigated using X-ray diffraction (XRD) and scanning electron microscopy (SEM). Results indicated the change of loss of ductility with temperature and the maximum loss of ductility was observed at 448 K (175 °C). XRD studies of the specimens revealed the formation of iron carbonate on the surface. SEM study of the surface of the specimens showed a rhombohedric crystalline iron carbonate layer above 373 K (100 °C), while no FeCO3 was detected at temperatures below 373 K (100 °C). Also, the crack size and depth of the cracks increased with temperature.

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Notes

  1. INCONEL is a trademark of Special Metals Corporation, New Hartford, NY.

  2. PHILIPS is a trademark of FEI Company, Hillsboro, OR.

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Acknowledgments

The authors express their appreciation for the support of the Petroleum Institute, Abu Dhabi, United Arab Emirates. They are also thankful to Devasco International Inc. (Welding Products) for their help and support.

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Authors and Affiliations

  1. Metallurgical and Materials Engineering Department, Colorado School of Mines, Golden, CO, 80401, USA

    Arshad Bajvani Gavanluei (Material Science PhD Candidate) & Brajendra Mishra (Professor and Associate Head)

  2. Materials Science Program, Colorado School of Mines, Golden, CO, 80401, USA

    David L. Olson (Professor and Lead Scientist)

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  1. Arshad Bajvani Gavanluei
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  2. Brajendra Mishra
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  3. David L. Olson
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Correspondence to Arshad Bajvani Gavanluei.

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Manuscript submitted March 21, 2011.

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Bajvani Gavanluei, A., Mishra, B. & Olson, D.L. Effect of Temperature on the Loss of Ductility of S-135 Grade Drill Pipe Steel and Characterization of Corrosion Products in CO2 Containing Environments. Metall Mater Trans A 43, 2850–2856 (2012). https://doi.org/10.1007/s11661-011-0777-x

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