Abstract
A suite of three green tea-containing Standard Reference Materials (SRMs) has been issued by the National Institute of Standards and Technology (NIST): SRM 3254 Camellia sinensis (Green Tea) Leaves, SRM 3255 Camellia sinensis (Green Tea) Extract, and SRM 3256 Green Tea-Containing Solid Oral Dosage Form. The materials are characterized for catechins, xanthine alkaloids, theanine, and toxic elements. As many as five methods were used in assigning certified and reference values to the constituents, with measurements carried out at NIST and at collaborating laboratories. The materials are intended for use in the development and validation of new analytical methods, and for use as control materials as a component in the support of claims of metrological traceability.
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Neilson AP, Green RJ, Wood KV, Ferruzzi MG (2006) J Chromatogr A 1132:132–140
Hu B, Wang L, Zhou B, Zhang X, Sun Y, Ye H, Zhao LY, Hu QH, Wang GX, Zeng XX (2009) J Chromatogr A 1216:3223–3231
Hussain I, Khan H, Saleem M, Marwat GA, Iqbal Y (2008) J Chem Soc Pak 30:571–576
Mizukami Y, Sawai Y, Yamaguchi Y (2007) J Agric Food Chem 55:4957–4964
Saito ST, Froehlich PE, Gosmann G, Bergold AM (2007) Chromatographia 65:607–610
Blahova E, Lehotay J (2006) Chem Anal 51:795–807
Repolles C, Herrero-Martinez JM, Rafols C (2006) J Chromatogr A 1131:51–57
Hong SB, Kim JI, Row KH (2002) Separ Sci Tech 37:1631–1640
Dalluge JJ, Nelson BC, Brown Thomas JM, Sander LC (1998) J Chromatogr A 793:265–274
Amarowicz R, Shahidi F (1996) Food Res Int 29:71–76
Goto T, Yoshida Y, Kiso M, Nagashima H (1996) J Chromatogr A 749:295–299
Pongsuwan W, Bamba T, Harada K, Yonetani T, Kobayashi A, Fukusaki E (2008) J Agric Food Chem 56:10705–10708
Mata-Bilbao MDL, Andres-Lacueva C, Roura E, Jauregui O, Torre C, Lamuela-Raventos RM (2007) J Agric Food Chem 55:8857–8863
Masukawa Y, Matsui Y, Shimizu N, Kondou N, Endou H, Kuzukawa M, Hase T (2006) J Chromat B Biomed Sci Appl 834:26–34
Frauen M, Rode T, Rapp C, Steinhart H (2002) Chromatographia 55:43–48
Dalluge JJ, Nelson BC, Brown Thomas JM, Welch MJ, Sander LC (1997) Rapid Commun Mass Spectrom 11:1753–1756
Chu KO, Wang CC, Rogers MS, Choy KW, Pang CP (2004) Anal Chim Acta 510:69–76
Lee MJ, Prabhu S, Meng XF, Li C, Yang CS (2000) Anal Biochem 279:164–169
Chen QS, Zhao JW, Chaitep SP, Guo ZM (2009) Food Chem 113:1272–1277
Robb CS, Geldart SE, Seelenbinder JA, Brown PR (2002) J Liq Chromatogr Relat Technol 25:787–801
Dalluge JJ, Nelson BC (2000) J Chromatogr A 881:411–424
Bonoli M, Pelillo M, Toschi TG, Lercker G (2003) Food Chem 81:631–638
Chu KO, Wang CC, Chu CY, Rogers MS, Choy KW, Pang CP (2004) J Chromatogr B 810:187–195
Pelillo M, Bonoli M, Biguzzi B, Bendini A, Toschi TG, Lercker G (2004) Food Chem 87:465–470
Sharma V, Gulati A, Ravindranath SD, Kumar V (2005) J Food Compos Anal 18:583–594
Wang HF, Provan GJ, Helliwell K (2003) Food Chem 81:307–312
Spacil Z, Novakova L, Solich P (2010) Food Chem 123:535–541
Peng ZK, Hayasaka Y, Iland PG, Sefton M, Hoj P, Waters EJ (2001) J Agric Food Chem 49:26–31
Kotani A, Miyashita N, Kusu F (2003) J Chromat B Biomed Sci Appl 788:269–275
Nishitani E, Sagesaka YM (2004) J Food Compos Anal 17:675–685
Yang DJ, Hwang LS, Lin JT (2007) J Chromatogr A 1156:312–320
Wang DM, Lu JL, Miao AQ, Xie ZY, Yang DP (2008) J Food Compos Anal 21:361–369
Aucamp JP, Hara Y, Apostolides Z (2000) J Chromatogr A 876:235–242
Bonoli M, Colabufalo P, Pelillo M, Toschi TG, Lercker G (2003) J Agric Food Chem 51:1141–1147
Nelson BC, Brown Thomas JM, Wise SA, Dalluge JJ (1998) J Microcolumn Sep 10:671–679
Stach D, Schmitz OJ (2001) J Chromatogr A 924:519–522
Watanabe T, Nishiyama R, Yamamoto A, Nagai S, Terabe S (1998) Anal Sci 14:435–438
Weiss DJ, Anderton CR (2003) J Chromatogr A 1011:173–180
Worth CCT, Wiessler M, Schmitz OJ (2000) Electrophoresis 21:3634–3638
Weiss DJ, Austria EJ, Anderton CR, Hompesch R, Jander A (2006) J Chromatogr A 1117:103–108
Li ZB, Huang DN, Tang ZX, Deng CH (2010) J Sep Sci 33:1079–1084
Gu XG, Cai JB, Zhang ZZ, Su QD (2007) Ann Chim 97:321–330
Friedman M, Levin CE, Choi SH, Kozukue E, Kozukue N (2006) J Food Sci 71:C328–C337
Cheong WJ, Park MH, Kang GW, Ko JH, Seo YJ (2005) Bull Kor Chem Soc 26:747–754
Pineiro Z, Palma M, Barroso CG (2004) J Chromatogr A 1026:19–23
Song GQ, Lin JM, Qu F, Huie CW (2003) Chin Sci Bull 48:2438–2443
Chang CJ, Chiu KL, Chen YL, Yang PW (2001) J Food Compos Anal 14:75–82
Suematsu S, Hisanobu Y, Saigo H, Matsuda R, Hara K, Komatsu Y (1992) J Jpn Soc Food Sci Technol 39:178–182
Dangerous Supplements: What you don’t know about these 12 ingredients could hurt you. http://www.consumerreports.org/health/natural-health/dietary-supplements/overview/index.htm. 2010
Dietary Supplement Health and Education Act (1994) Public Law 103–417 [S.784]; Oct 25
Food and Drug Administration (2007) Fed Regist 72:34751–34958
JCGM (2008) International vocabulary of metrology - basic and general concepts and associated terms. VIM, Bureau International des Poids et Mesures
Bedner M, Duewer DL (2011) Anal Chem 83:6169–6176
ASTM Standard D6722-01 (2006) Standard Test Method for Total Mercury in Coal and Coal Combustion Residues by Direct Combustion Analysis. ASTM International, West Conshohocken, PA, doi:10.1520/D6722-01R06, www.astm.org
Christopher SJ, Long SE, Rearick MS, Fassett JD (2001) Anal Chem 73:2190–2199
Baer I, de la Calle Guntinas MB, Sander LC, Long S, Christopher SJ, Day RD, Murphy KE, Verbist I, Vendelbo D, Emteborg H, Taylor P (2009) IMEP-28: Total Arsenic, Cadmium, Lead and Mercury in Food Supplements. JRC Scientific and Technical Reports JRC55721, 1–46
de la Calle Guntinas MB, Sander LC, Long SE, Christopher SJ, Day RD, Murphy KE, Cordeiro Raposo F, Linsinger T, Emteborg H, Verbist I, Vendelbo D (2009) Report of the Sixth Interlaboratory Comparison Organised by the Community Reference Laboratory for Heavy Metals in Feed and Food - Total Cd, Pb, As and Hg in Food Supplements. JRC Scientific and Technical Reports JRC54402, 1–42. 9-24-2009.
Sander LC, Putzbach K, Nelson BC, Rimmer CA, Bedner M, Thomas JB, Porter B, Wood LJ, Schantz MM, Murphy KE, Sharpless KE, Wise SA, Yen JH, Siitonnen PH, NguyenPho A, Roman MC, Betz JM (2008) Anal Bioanal Chem 391:2023–2034
Peng L, Song XH, Shi XG, Li JX, Ye CX (2008) J Food Compos Anal 21:559–563
Pelillo M, Biguzzi B, Bendini A, Toschi TG, Vanzini M, Lercker G (2002) Food Chem 78:369–374
Bedner M, Sander LC, Sharpless KE (2010) Anal Bioanal Chem 397:1773–1777
Poster DL, Kucklick JR, Schantz MM, Porter BJ, Leigh SD, Wise SA (2003) Anal Bioanal Chem 375:223–241
Acknowledgement
Partial funding for this work was provided by the National Institutes of Health, Office of Dietary Supplements. M. Schantz and E. McGaw (NIST) are acknowledged for pesticide screening of the three SRMs.
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Published in the 10th Anniversary Issue.
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Sander, L.C., Bedner, M., Tims, M.C. et al. Development and certification of green tea-containing standard reference materials. Anal Bioanal Chem 402, 473–487 (2012). https://doi.org/10.1007/s00216-011-5472-7
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DOI: https://doi.org/10.1007/s00216-011-5472-7