Skip to main content
Log in

Development and certification of green tea-containing standard reference materials

  • Original Paper
  • Published:
Analytical and Bioanalytical Chemistry Aims and scope Submit manuscript

Abstract

A suite of three green tea-containing Standard Reference Materials (SRMs) has been issued by the National Institute of Standards and Technology (NIST): SRM 3254 Camellia sinensis (Green Tea) Leaves, SRM 3255 Camellia sinensis (Green Tea) Extract, and SRM 3256 Green Tea-Containing Solid Oral Dosage Form. The materials are characterized for catechins, xanthine alkaloids, theanine, and toxic elements. As many as five methods were used in assigning certified and reference values to the constituents, with measurements carried out at NIST and at collaborating laboratories. The materials are intended for use in the development and validation of new analytical methods, and for use as control materials as a component in the support of claims of metrological traceability.

Green Tea - Camellia sinensis

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4

Similar content being viewed by others

References

  1. Neilson AP, Green RJ, Wood KV, Ferruzzi MG (2006) J Chromatogr A 1132:132–140

    Article  CAS  Google Scholar 

  2. Hu B, Wang L, Zhou B, Zhang X, Sun Y, Ye H, Zhao LY, Hu QH, Wang GX, Zeng XX (2009) J Chromatogr A 1216:3223–3231

    Article  CAS  Google Scholar 

  3. Hussain I, Khan H, Saleem M, Marwat GA, Iqbal Y (2008) J Chem Soc Pak 30:571–576

    CAS  Google Scholar 

  4. Mizukami Y, Sawai Y, Yamaguchi Y (2007) J Agric Food Chem 55:4957–4964

    Article  CAS  Google Scholar 

  5. Saito ST, Froehlich PE, Gosmann G, Bergold AM (2007) Chromatographia 65:607–610

    CAS  Google Scholar 

  6. Blahova E, Lehotay J (2006) Chem Anal 51:795–807

    CAS  Google Scholar 

  7. Repolles C, Herrero-Martinez JM, Rafols C (2006) J Chromatogr A 1131:51–57

    Article  CAS  Google Scholar 

  8. Hong SB, Kim JI, Row KH (2002) Separ Sci Tech 37:1631–1640

    Article  CAS  Google Scholar 

  9. Dalluge JJ, Nelson BC, Brown Thomas JM, Sander LC (1998) J Chromatogr A 793:265–274

    Article  CAS  Google Scholar 

  10. Amarowicz R, Shahidi F (1996) Food Res Int 29:71–76

    Article  CAS  Google Scholar 

  11. Goto T, Yoshida Y, Kiso M, Nagashima H (1996) J Chromatogr A 749:295–299

    Article  CAS  Google Scholar 

  12. Pongsuwan W, Bamba T, Harada K, Yonetani T, Kobayashi A, Fukusaki E (2008) J Agric Food Chem 56:10705–10708

    Article  CAS  Google Scholar 

  13. Mata-Bilbao MDL, Andres-Lacueva C, Roura E, Jauregui O, Torre C, Lamuela-Raventos RM (2007) J Agric Food Chem 55:8857–8863

    Article  CAS  Google Scholar 

  14. Masukawa Y, Matsui Y, Shimizu N, Kondou N, Endou H, Kuzukawa M, Hase T (2006) J Chromat B Biomed Sci Appl 834:26–34

    Article  CAS  Google Scholar 

  15. Frauen M, Rode T, Rapp C, Steinhart H (2002) Chromatographia 55:43–48

    Article  CAS  Google Scholar 

  16. Dalluge JJ, Nelson BC, Brown Thomas JM, Welch MJ, Sander LC (1997) Rapid Commun Mass Spectrom 11:1753–1756

    Article  CAS  Google Scholar 

  17. Chu KO, Wang CC, Rogers MS, Choy KW, Pang CP (2004) Anal Chim Acta 510:69–76

    Article  CAS  Google Scholar 

  18. Lee MJ, Prabhu S, Meng XF, Li C, Yang CS (2000) Anal Biochem 279:164–169

    Article  CAS  Google Scholar 

  19. Chen QS, Zhao JW, Chaitep SP, Guo ZM (2009) Food Chem 113:1272–1277

    Article  CAS  Google Scholar 

  20. Robb CS, Geldart SE, Seelenbinder JA, Brown PR (2002) J Liq Chromatogr Relat Technol 25:787–801

    Article  CAS  Google Scholar 

  21. Dalluge JJ, Nelson BC (2000) J Chromatogr A 881:411–424

    Article  CAS  Google Scholar 

  22. Bonoli M, Pelillo M, Toschi TG, Lercker G (2003) Food Chem 81:631–638

    Article  CAS  Google Scholar 

  23. Chu KO, Wang CC, Chu CY, Rogers MS, Choy KW, Pang CP (2004) J Chromatogr B 810:187–195

    CAS  Google Scholar 

  24. Pelillo M, Bonoli M, Biguzzi B, Bendini A, Toschi TG, Lercker G (2004) Food Chem 87:465–470

    Article  CAS  Google Scholar 

  25. Sharma V, Gulati A, Ravindranath SD, Kumar V (2005) J Food Compos Anal 18:583–594

    Article  CAS  Google Scholar 

  26. Wang HF, Provan GJ, Helliwell K (2003) Food Chem 81:307–312

    Article  CAS  Google Scholar 

  27. Spacil Z, Novakova L, Solich P (2010) Food Chem 123:535–541

    Article  CAS  Google Scholar 

  28. Peng ZK, Hayasaka Y, Iland PG, Sefton M, Hoj P, Waters EJ (2001) J Agric Food Chem 49:26–31

    Article  CAS  Google Scholar 

  29. Kotani A, Miyashita N, Kusu F (2003) J Chromat B Biomed Sci Appl 788:269–275

    Article  CAS  Google Scholar 

  30. Nishitani E, Sagesaka YM (2004) J Food Compos Anal 17:675–685

    Article  CAS  Google Scholar 

  31. Yang DJ, Hwang LS, Lin JT (2007) J Chromatogr A 1156:312–320

    Article  CAS  Google Scholar 

  32. Wang DM, Lu JL, Miao AQ, Xie ZY, Yang DP (2008) J Food Compos Anal 21:361–369

    Article  CAS  Google Scholar 

  33. Aucamp JP, Hara Y, Apostolides Z (2000) J Chromatogr A 876:235–242

    Article  CAS  Google Scholar 

  34. Bonoli M, Colabufalo P, Pelillo M, Toschi TG, Lercker G (2003) J Agric Food Chem 51:1141–1147

    Article  CAS  Google Scholar 

  35. Nelson BC, Brown Thomas JM, Wise SA, Dalluge JJ (1998) J Microcolumn Sep 10:671–679

    Article  CAS  Google Scholar 

  36. Stach D, Schmitz OJ (2001) J Chromatogr A 924:519–522

    Article  CAS  Google Scholar 

  37. Watanabe T, Nishiyama R, Yamamoto A, Nagai S, Terabe S (1998) Anal Sci 14:435–438

    Article  CAS  Google Scholar 

  38. Weiss DJ, Anderton CR (2003) J Chromatogr A 1011:173–180

    Article  CAS  Google Scholar 

  39. Worth CCT, Wiessler M, Schmitz OJ (2000) Electrophoresis 21:3634–3638

    Article  CAS  Google Scholar 

  40. Weiss DJ, Austria EJ, Anderton CR, Hompesch R, Jander A (2006) J Chromatogr A 1117:103–108

    Article  CAS  Google Scholar 

  41. Li ZB, Huang DN, Tang ZX, Deng CH (2010) J Sep Sci 33:1079–1084

    CAS  Google Scholar 

  42. Gu XG, Cai JB, Zhang ZZ, Su QD (2007) Ann Chim 97:321–330

    Article  CAS  Google Scholar 

  43. Friedman M, Levin CE, Choi SH, Kozukue E, Kozukue N (2006) J Food Sci 71:C328–C337

    Article  CAS  Google Scholar 

  44. Cheong WJ, Park MH, Kang GW, Ko JH, Seo YJ (2005) Bull Kor Chem Soc 26:747–754

    Article  CAS  Google Scholar 

  45. Pineiro Z, Palma M, Barroso CG (2004) J Chromatogr A 1026:19–23

    Article  CAS  Google Scholar 

  46. Song GQ, Lin JM, Qu F, Huie CW (2003) Chin Sci Bull 48:2438–2443

    CAS  Google Scholar 

  47. Chang CJ, Chiu KL, Chen YL, Yang PW (2001) J Food Compos Anal 14:75–82

    Article  CAS  Google Scholar 

  48. Suematsu S, Hisanobu Y, Saigo H, Matsuda R, Hara K, Komatsu Y (1992) J Jpn Soc Food Sci Technol 39:178–182

    CAS  Google Scholar 

  49. Dangerous Supplements: What you don’t know about these 12 ingredients could hurt you. http://www.consumerreports.org/health/natural-health/dietary-supplements/overview/index.htm. 2010

  50. Dietary Supplement Health and Education Act (1994) Public Law 103–417 [S.784]; Oct 25

  51. Food and Drug Administration (2007) Fed Regist 72:34751–34958

    Google Scholar 

  52. JCGM (2008) International vocabulary of metrology - basic and general concepts and associated terms. VIM, Bureau International des Poids et Mesures

    Google Scholar 

  53. Bedner M, Duewer DL (2011) Anal Chem 83:6169–6176

    Article  CAS  Google Scholar 

  54. ASTM Standard D6722-01 (2006) Standard Test Method for Total Mercury in Coal and Coal Combustion Residues by Direct Combustion Analysis. ASTM International, West Conshohocken, PA, doi:10.1520/D6722-01R06, www.astm.org

  55. Christopher SJ, Long SE, Rearick MS, Fassett JD (2001) Anal Chem 73:2190–2199

    Article  CAS  Google Scholar 

  56. Baer I, de la Calle Guntinas MB, Sander LC, Long S, Christopher SJ, Day RD, Murphy KE, Verbist I, Vendelbo D, Emteborg H, Taylor P (2009) IMEP-28: Total Arsenic, Cadmium, Lead and Mercury in Food Supplements. JRC Scientific and Technical Reports JRC55721, 1–46

  57. de la Calle Guntinas MB, Sander LC, Long SE, Christopher SJ, Day RD, Murphy KE, Cordeiro Raposo F, Linsinger T, Emteborg H, Verbist I, Vendelbo D (2009) Report of the Sixth Interlaboratory Comparison Organised by the Community Reference Laboratory for Heavy Metals in Feed and Food - Total Cd, Pb, As and Hg in Food Supplements. JRC Scientific and Technical Reports JRC54402, 1–42. 9-24-2009.

  58. Sander LC, Putzbach K, Nelson BC, Rimmer CA, Bedner M, Thomas JB, Porter B, Wood LJ, Schantz MM, Murphy KE, Sharpless KE, Wise SA, Yen JH, Siitonnen PH, NguyenPho A, Roman MC, Betz JM (2008) Anal Bioanal Chem 391:2023–2034

    Article  CAS  Google Scholar 

  59. Peng L, Song XH, Shi XG, Li JX, Ye CX (2008) J Food Compos Anal 21:559–563

    Article  CAS  Google Scholar 

  60. Pelillo M, Biguzzi B, Bendini A, Toschi TG, Vanzini M, Lercker G (2002) Food Chem 78:369–374

    Article  CAS  Google Scholar 

  61. Bedner M, Sander LC, Sharpless KE (2010) Anal Bioanal Chem 397:1773–1777

    Article  CAS  Google Scholar 

  62. Poster DL, Kucklick JR, Schantz MM, Porter BJ, Leigh SD, Wise SA (2003) Anal Bioanal Chem 375:223–241

    CAS  Google Scholar 

Download references

Acknowledgement

Partial funding for this work was provided by the National Institutes of Health, Office of Dietary Supplements. M. Schantz and E. McGaw (NIST) are acknowledged for pesticide screening of the three SRMs.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to L. C. Sander.

Additional information

Contribution of the National Institute of Standards and Technology. Not subject to copyright.

Published in the 10th Anniversary Issue.

Electronic supplementary material

Below is the link to the electronic supplementary material.

ESM 1

(PDF 1.97 mb)

Rights and permissions

Reprints and permissions

About this article

Cite this article

Sander, L.C., Bedner, M., Tims, M.C. et al. Development and certification of green tea-containing standard reference materials. Anal Bioanal Chem 402, 473–487 (2012). https://doi.org/10.1007/s00216-011-5472-7

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s00216-011-5472-7

Keywords

Navigation