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Microphotometric determination of 1-dimethylaminonaphthalene-5-sulfonylamino acids with glycine as an example

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Chemistry of Natural Compounds Aims and scope

Conclusions

1. A method for the quantitative evaluation of thin-layer chromatograms of dansylglycine by photographing them and microphotometering the negative obtained has been proposed.

2. The method is applicable to amounts of 1·10−10–1·10−9 mole of dansylglycine per spot with an accuracy of ±3%.

3. It is proposed to obtain dansyl amino acids by using dioxane as solvent, which completely prevents the parasitic formation of dansylamide.

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References

  1. W. R. Gray and B. S. Hartley, Biochem. J., 89, 590, 1963.

    Article  Google Scholar 

  2. N. Seiler and M. Wiechmann, Z. anal. Chem., 220, 109, 1966.

    Article  CAS  Google Scholar 

  3. G. Pataki and E. Strasky, Chimia, 20, 361, 1966.

    CAS  Google Scholar 

  4. N. Seiler, G. Werner, and M. Wiechmann, Naturw., 50, 643, 1963.

    Article  CAS  Google Scholar 

  5. S. R. Mardashev, M. Z. Zalesskii, S. I. Pekhtereva, and L. A. Semina, Biokhim., 32, 655, 1967.

    CAS  Google Scholar 

  6. D. J. Neadle and R. J. Pollitt, Biochim. J., 97, 607, 1965.

    Article  CAS  Google Scholar 

  7. N. Seiler and M. Wiechmann, J. Chromatog., 28, 351, 1967.

    Article  CAS  Google Scholar 

  8. B. G. Belen'kii, E. S. Gankina, and V. V. Nesterov, DAN SSSR, 172, 91, 1967.

    CAS  Google Scholar 

  9. V. P. Mikulin, Handbook of Photographic Formulations [in Russian], Moscow, 113, 1960.

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Authors and Affiliations

  1. Zelinskii Institute of Organic Chemistry, AS USSR, USSR

    V. Kh. Lapuk, A. A. Strongina & M. Z. Zalesskii

Authors
  1. V. Kh. Lapuk
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  2. A. A. Strongina
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  3. M. Z. Zalesskii
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Additional information

Khimiya Prirodnykh Soedinenii, Vol. 5, No. 6, pp. 531–535, 1969

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Lapuk, V.K., Strongina, A.A. & Zalesskii, M.Z. Microphotometric determination of 1-dimethylaminonaphthalene-5-sulfonylamino acids with glycine as an example. Chem Nat Compd 5, 450–452 (1969). https://doi.org/10.1007/BF00568588

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  • DOI: https://doi.org/10.1007/BF00568588

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