Summary
The acetate of bisnorlithocholic acid has been obtained with a yield of 65% from the acetate of 5β-ergost-22-en-3α-ol by permanganate-periodate oxidation.
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D. A. Shepherd, R. A. Donia, J. A. Campbell, B. A. Johnson, R. P. Holysz, G. Slomp, Jr., J. E. Stafford, R. Z. Pederson, and A. C. Ott, J. Am. Chem. Soc.,77, 1212 (1955).
J. Johnson, G. T. Newbold, and F. S. Spring, J. Chem. Soc., 1302 (1954).
US Patent No. 3,444,216 (1969); Chem. Abstr.,71, 50375n (1970).
J. P. Moreau, D. J. Aberhart, and E. Caspi, J. Org. Chem.,39, 2018 (1974).
A. J. Fatiadi, Syntheses,4, 229;4, 253 (1974).
V. A. Rulin, V. F. Shner, and N. N. Suvorov, Khim. Prirodn. Soedin., 676 (1974).
F. Johnson, G. T. Newbold, and F. S. Spring, Chem. Ind. (London), 1230 (1953).
R. Reich and J. F. W. Keana, Synth. Commun.,2, (5), 323 (1972).
N. N. Suvorov, Med. Prom., No. 10, 22 (1956).
E. Fernholz, Ann. Chem.,507, 128 (1933).
Additional information
S. Ordzhonikidze All-Union Scientific-Research Institute of Pharmaceutical Chemistry, Moscow. Translated from Khimiya Prirodnykh Soedinenii, No. 1, pp. 88–91, January–February, 1978.
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Popova, E.V., Anisimova, O.S., Arsent'ev, A.G. et al. Oxidation of the side chains of ergosterol derivatives. Chem Nat Compd 14, 70–72 (1978). https://doi.org/10.1007/BF00565880
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DOI: https://doi.org/10.1007/BF00565880