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Mass-spectrometric analysis of complex volatile and nonvolatile crude oil components: a challenge

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Abstract

Crude oil analysis has long been an inspiration for the development of analytical techniques. Especially mass spectrometry has flourished as a result of the challenge these extremely complex problems offer. Here an overview of different analytical methods is presented that shows different ways to analyze volatile and nonvolatile crude oil components. Focus has been placed on the use of mass spectrometry and especially the new developments that have been introduced using the emerging technique of Fourier transform ion cyclotron resonance mass spectrometry. These studies are examples of how far the development of analytical methods has come for the task of studying such complex problems.

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References

  1. Maugeri L (2004) Science 304:1114–1115

    Article  CAS  Google Scholar 

  2. Barman BN, Cebolla VL, Membrado L (2000) Crit Rev Anal Chem 30:75–120

    Article  CAS  Google Scholar 

  3. Marshall AG, Rodgers RP (2004) Acc Chem Res 37:53–59

    Article  CAS  Google Scholar 

  4. Albert DK (1967) Anal Chem 39:1113–1117

    Article  CAS  Google Scholar 

  5. Albert DK (1978) Anal Chem 50:1822–1829

    Article  CAS  Google Scholar 

  6. Bradley C, Schiller DJ (1986) Anal Chem 58:3017–3021

    Article  CAS  Google Scholar 

  7. Martin RL, Grant JA (1965) Anal Chem 37:644–649

    Article  CAS  Google Scholar 

  8. Schade T, Andersson JT (2006) Energy Fuels 20:1614–1620

    Article  CAS  Google Scholar 

  9. Schade T, Roberz B, Andersson JT (2002) Polycyclic Aromat Compd 22:311–320

    Article  CAS  Google Scholar 

  10. Schwartz RD, Brasseaux DJ (1963) Anal Chem 35:1374–1382

    Article  CAS  Google Scholar 

  11. Swansige JT, Dickson FE (1973) Anal Chem 45:811–813

    Article  Google Scholar 

  12. Gough MA, Rowland SJ (1990) Nature 344:648–650

    Article  CAS  Google Scholar 

  13. Blomberg J, Schoenmakers PJ, Beens J, Tijssen R (1997) J High Resolut Chromatogr 20:539–544

    Article  CAS  Google Scholar 

  14. Beens J, Blomberg J, Schoenmakers PJ (2000) J High Resolut Chromatogr 23:182–188

    Article  CAS  Google Scholar 

  15. Frysinger GS, Gaines RB (1999) J High Resolut Chromatogr 22:251–255

    Article  CAS  Google Scholar 

  16. Frysinger GS, Gaines RB, Xu L, Reddy CM (2003) Environ Sci Technol 37:1653–1662

    Article  CAS  Google Scholar 

  17. Hua RX, Wang JH, Kong HW, Liu J, Lu X, Xu GW (2004) J Sep Sci 27:691–698

    Article  CAS  Google Scholar 

  18. von Muhlen C, Zini CA, Caramao EB, Marriott PJ (2006) J Chromatogr A 1105:39–50

    Article  Google Scholar 

  19. Choudhary TV, Malandra J, Green J, Parrott S, Johnson B (2006) Angew Chem Int Ed 45:3299–3303

    Article  CAS  Google Scholar 

  20. Quimby BD, Dryden PC, Sullivan JJ (1991) J High Resolut Chromatogr 14:110–116

    Article  CAS  Google Scholar 

  21. Zeng YD, Uden PC (1994) J High Resolut Chromatgr 17:223–229

    Article  CAS  Google Scholar 

  22. Davies IL, Bartle KD, Andrews GE, Williams PT (1988) J Chromatogr Sci 26:125–130

    Article  CAS  Google Scholar 

  23. Mössner SG, Wise SA (1999) Anal Chem 71:58–69

    Article  Google Scholar 

  24. Wise SA, Chesler SN, Hertz HS, Hilpert LR, May WE (1977) Anal Chem 49:2306–2310

    Article  CAS  Google Scholar 

  25. Felix G, Bertrand C (1984) J High Resolut Chromatogr Chromatogr Commun 7:160–161

    Article  CAS  Google Scholar 

  26. Holstein W (1981) Chromatographia 14:468–477

    Article  CAS  Google Scholar 

  27. Kershaw JR, Black KJT (1993) Energy Fuels 7:420–425

    Article  CAS  Google Scholar 

  28. Ma XL, Sakanishi K, Isoda T, Mochida I (1997) Fuel 76:329–339

    Article  CAS  Google Scholar 

  29. Hegazi AH, Andersson JT (2007) Energy Fuels (in press)

  30. Bouyssiere B, Leonhard P, Profrock D, Baco F, Garcia CL, Wilbur S, Prange A (2004) J Anal At Spectrom 19:700–702

    Article  CAS  Google Scholar 

  31. Boulyga SF, Heilmann J, Heumann KG (2005) Anal Bioanal Chem 382:1808–1814

    Article  CAS  Google Scholar 

  32. Heilmann J, Boulyga SF, Heumann KG (2004) Anal Bioanal Chem 380:190–197

    Article  CAS  Google Scholar 

  33. Boduszynski MM (1987) Energy Fuels 1:2–11

    Article  CAS  Google Scholar 

  34. Comisarow MB, Marshall AG (1974) Chem Phys Lett 25:282–283

    Article  CAS  Google Scholar 

  35. Makarov A, Denisov E, Lange O, Kholomeev A, Horning S (2005) In: Proceedings of the 53rd ASMS conference on mass spectrometry and allied topics, San Antonio, 5–9 June 2005

  36. Kim S, Rodgers RP, Marshall AG (2006) Int J Mass Spectrom 251:260–265

    Article  CAS  Google Scholar 

  37. Marshall AG, Hendrickson CL (2002) Int J Mass Spectrom 215:59–75

    Article  CAS  Google Scholar 

  38. Marshall AG, Hendrickson CL, Jackson GS (1998) Mass Spectrom Rev 17:1–35

    Article  CAS  Google Scholar 

  39. Schrader W, Klein HW (2004) Anal Bioanal Chem 379:1013–1024

    Article  CAS  Google Scholar 

  40. Field FH, Hastings SH (1956) Anal Chem 28:1248–1255

    Article  CAS  Google Scholar 

  41. Qian K, Hsu CS (1992) Anal Chem 64:2327–2333

    Article  CAS  Google Scholar 

  42. Hsu CS, Qian KG (1993) Anal Chem 65:767–771

    Article  CAS  Google Scholar 

  43. Roussis SG, Fitzgerald WP, Cameron AS (1998) Rapid Commun Mass Spectrom 12:373–381

    Article  CAS  Google Scholar 

  44. Creaser CS, Krokos F, Oneill KE, Smith MJC, Mcdowell PG (1993) J Am Soc Mass Spectrom 4:322–326

    Article  CAS  Google Scholar 

  45. Hsu CS, Qian KN, Robbins WK (1994) J High Resolut Chromatogr 17:271–276

    Article  CAS  Google Scholar 

  46. Guan SH, Marshall AG, Scheppele SE (1996) Anal Chem 68:46–71

    Article  CAS  Google Scholar 

  47. Fu JM, Purcell JM, Quinn JP, Schaub TM, Hendrickson CL, Rodgers RP, Marshall AG (2006) Rev Sci Instrum 77:025102/1–025102/9

    CAS  Google Scholar 

  48. Rodgers RP, White FM, Hendrickson CL, Marshall AG, Andersen KV (1998) Anal Chem 70:4743–4750

    Article  CAS  Google Scholar 

  49. Fu JM, Kim S, Rodgers RP, Hendrickson CL, Marshall AG, Qian KN (2006) Energy Fuels 20:661–667

    Article  CAS  Google Scholar 

  50. Crawford KE, Campbell JL, Fiddler MN, Duan P, Qian K, Gorbaty ML, Kenttamaa HI (2005) Anal Chem 77:7916–7923

    Article  CAS  Google Scholar 

  51. Shea RC, Habicht SC, Vaughn WE, Kenttamaa HI (2007) Anal Chem 79:2688–2694

    Article  CAS  Google Scholar 

  52. Fenn JB, Mann M, Meng CK, Wong SF, Whitehouse CM (1989) Science 246:64–71

    Article  CAS  Google Scholar 

  53. Zhan DL, Fenn JB (2000) Int J Mass Spectrom 194:197–208

    Article  CAS  Google Scholar 

  54. Hughey CA, Hendrickson CL, Rodgers RP, Marshall AG (2001) Energy Fuels 15:1186–1193

    Article  CAS  Google Scholar 

  55. Hughey CA, Rodgers RP, Marshall AG (2002) Anal Chem 74:4145–4149

    Article  CAS  Google Scholar 

  56. Hughey CA, Rodgers RP, Marshall AG, Qian KN, Robbins WK (2002) Org Geochem 33:743–759

    Article  CAS  Google Scholar 

  57. Wu ZG, Rodgers RP, Marshall AG (2004) Energy Fuels 18:1424–1428

    Article  CAS  Google Scholar 

  58. Hughey CA, Rodgers RP, Marshall AG, Walters CC, Qian KN, Mankiewicz P (2004) Org Geochem 35:863–880

    Article  CAS  Google Scholar 

  59. Kim S, Stanford LA, Rodgers RP, Marshall AG, Walters CC, Qian K, Wenger LM, Mankiewicz P (2005) Org Geochem 36:1117–1134

    Article  CAS  Google Scholar 

  60. Qian KN, Robbins WK, Hughey CA, Cooper HJ, Rodgers RP, Marshall AG (2001) Energy Fuels 15:1505–1511

    Article  CAS  Google Scholar 

  61. Rudzinski WE, Oehlers L, Zhang Y (2002) Energy Fuels 16:1178–1185

    Article  CAS  Google Scholar 

  62. Barrow MP, McDonnell LA, Feng XD, Walker J, Derrick PJ (2003) Anal Chem 75:860–866

    Article  CAS  Google Scholar 

  63. Gabryelski W, Froese KL (2003) Anal Chem 75:4612–4623

    Article  CAS  Google Scholar 

  64. Hockaday WC, Grannas AM, Kim S, Hatcher PG (2006) Org Geochem 37:501–510

    Article  CAS  Google Scholar 

  65. Qian K, Edwards KE, Diehl JH, Green LA (2004) Energy Fuels 18:1784–1791

    Article  CAS  Google Scholar 

  66. Roussis SG, Proulx R (2002) Anal Chem 74:1408–1414

    Article  CAS  Google Scholar 

  67. Rudzinski WE, Zhang Y, Luo XM (2003) J Mass Spectrom 38:167–173

    Article  CAS  Google Scholar 

  68. Müller H, Andersson JT, Schrader W (2005) Anal Chem 77:2536–2543

    Article  Google Scholar 

  69. Panda SK, Schrader W, Andersson JT (2006) J Chromatogr A 1122:88–96

    Article  CAS  Google Scholar 

  70. Panda SK, Schrader W, al-Hajji A, Andersson JT (2007) Energy Fuels 21:1071–1077

    Article  CAS  Google Scholar 

  71. Herod AA, Lazaro MJ, Rahman M, Domin M, Cocksedge MJ, Kandiyoti R (1997) Rapid Commun Mass Spectrom 11:1627–1634

    Article  CAS  Google Scholar 

  72. Artok L, Su Y, Hirose Y, Hosokawa M, Murata S, Nomura M (1999) Energy Fuels 13:287–296

    Article  CAS  Google Scholar 

  73. Artok L, Su Y, Hirose Y, Murata S, Nomura M (1999) Sekiyu Gakkaishi 42:206–214

    CAS  Google Scholar 

  74. Millan M, Behrouzi M, Karaca F, Morgan TJ, Herod AA, Kandiyoti R (2005) Catal Today 109:154–161

    Article  CAS  Google Scholar 

  75. Mueller H, Andersson J (2004) Polycyclic Aromat Compd 24:299–308

    Article  CAS  Google Scholar 

  76. Suelves I, Islas CA, Herod AA, Kandiyoti R (2001) Energy Fuels 15:429–437

    Article  CAS  Google Scholar 

  77. Robins C, Limbach PA (2003) Rapid Commun Mass Spectrom 17:2839–2845

    Article  CAS  Google Scholar 

  78. Rizzi A, Cosmina P, Flego C, Montanari L, Seraglia R, Traldi P (2006) J Mass Spectrom 41:1232–1241

    Article  CAS  Google Scholar 

  79. Qian KN, Edwards KE, Siskin M, Olmstead WN, Mennito AS, Dechert GJ, Hoosain NE (2007) Energy Fuels 21:1042–1047

    Article  CAS  Google Scholar 

  80. Boduszynski MM (1988) Energy Fuels 2:597–613

    Article  CAS  Google Scholar 

  81. Schaub TM, Hendrickson CL, Qian KN, Quinn JP, Marshall AG (2003) Anal Chem 75:2172–2176

    Article  CAS  Google Scholar 

  82. Schaub TM, Hendrickson CL, Quinn JP, Rodgers RP, Marshall AG (2005) Anal Chem 77:1317–1324

    Article  CAS  Google Scholar 

  83. Schaub TM, Rodgers RP, Marshall AG, Qian K, Green LA, Olmstead WN (2005) Energy Fuels 19:1566–1573

    Article  CAS  Google Scholar 

  84. Linden HB (2004) Eur J Mass Spectrom 10:459–468

    Article  CAS  Google Scholar 

  85. Schaub TM, Linden HB, Hendrickson CL, Marshall AG (2004) Rapid Commun Mass Spectrom 18:1641–1644

    Article  CAS  Google Scholar 

  86. Robb DB, Covey TR, Bruins AP (2000) Anal Chem 72:3653–3659

    Article  CAS  Google Scholar 

  87. Purcell JM, Hendrickson CL, Rodgers RP, Marshall AG (2006) Anal Chem 78:5906–5912

    Article  CAS  Google Scholar 

  88. Hsu CS, Qian KN, Chen YNC (1992) Anal Chim Acta 264:79–89

    Article  CAS  Google Scholar 

  89. McLafferty FW, Turecek F (1993) Interpretation of mass spectra. University Science Books, Sausalito

  90. Kendrick E (1963) Anal Chem 35:2146–2154

    Article  CAS  Google Scholar 

  91. Andersson JT, Panda SK, Schrader W (2007) In: ACS symposium series. American Chemical Society, Washington (in press)

  92. Rodgers RP, Schaub TM, Marshall AG (2005) Anal Chem 77:20A–27A

    Article  CAS  Google Scholar 

  93. Schaub TM, Rodgers RP, Marshall AG (2005) Energy Fuels 19:1566–1573

    Article  CAS  Google Scholar 

  94. van Krevelen DW (1950) Fuel 29:269–284

    Google Scholar 

  95. Kim S, Kramer RW, Hatcher PG (2003) Anal Chem 75:5336–5344

    Article  CAS  Google Scholar 

  96. Wu Z, Rodgers RP, Marshall AG (2004) Anal Chem 76:2511–2516

    Article  CAS  Google Scholar 

  97. Brown RA (1951) Anal Chem 23:430–437

    Article  CAS  Google Scholar 

Download references

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Correspondence to Wolfgang Schrader.

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Panda, S.K., Andersson, J.T. & Schrader, W. Mass-spectrometric analysis of complex volatile and nonvolatile crude oil components: a challenge. Anal Bioanal Chem 389, 1329–1339 (2007). https://doi.org/10.1007/s00216-007-1583-6

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  • DOI: https://doi.org/10.1007/s00216-007-1583-6

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