CommunicationFast MAS Total Through-Bond Correlation Spectroscopy☆
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2022, Journal of Magnetic ResonanceCitation Excerpt :As a result of these multiple features, numerous 13C–13C correlation experiments have been proposed where homonuclear interactions in spinning solids are reintroduced by manipulating the 1Hs that are present in the system; i.e., not the species whose correlations are being sought, but rather heteronuclear species that couple strongly to them. These include methods such as DARR, MIRROR, RAD, and AL-FRESCO, where 1Hs manipulations are timed with the MAS, so as to reinstate the effects of truncated 13C–13C (or 15N–15N) couplings [20–27]. While these experiments rely on dipolar couplings that are not meaningful in isotropic liquids, solution-phase counterparts might also exist where isotropic J couplings drive similar effects.
Functional and structural characterization of membrane-binding proteins using NMR
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Presented, in part, at the 41st ENC, Pacific Grove, CA.